AMRUT 1.0 Thrissur Corporation - Setting up of Pesticides and Heavy metals Lab

OD219871/2025-2026:Supply,Installation and commissioning ,testing training , provision of manpower for operating the instrument and shifting during warranty period of ICPMS with all accessories Specifications: A compact high sensitive ICP- MS system along with all accessories as per the specification given in the technical bid. Fully PC controlled system with compact size and bench top model should be able to determine major, minor and trace elements in water samples in single run measurement. Complete system should have extensive safety and service diagnostic facility Technical Specification ICP-MS 1.Application requirement The offered system must achieve at least 0.5 times of acceptable limits mentioned as follows Parameters Acceptable limit as per the standard 10500;2012 (Maximum) Parameters i.Aluminium as Al 0.03 mg/l ii.Barium as Ba 0.7 mg/l iii.Boron as B 0.5 mg/l iv.Calcium as Ca 75 mg/l v.Copper as Cu .05 mg/l vi. Iron as Fe 1.0 mg/l vii. Magnesium as Mg 30 mg/l viii.Manganese as Mn 0.1mg/l ix. Selenium as Se 0.01mg/l x. Silver as Ag 0.1mg/l xi. Zinc as Zn 5 mg/l xii. Cadmium as Cd 0.003 mg/l xiii. Lead as Pb 0.01 mg/l xiv. Mercury as Hg .001 mg/l xv. Molybdenum as Mo 0.07mg/l xvi. Nickel as Ni 0.02 mg/l xvii. Total Aresnic as As 0.01 mg/l xviii. Uranium 0.03mg/l xix.Total chromium as Cr 0.05 mg/l Instrument Design The instrument is the latest in the category and is capable of delivering ultra-trace analysis of elements at ppt level with adequate accuracy without changing any plasma parameter and in one single run for various sample matrices and through a PC controlled software. 2.Sample introduction system a. Sample Introduction Kit Spray Chamber (Temp Range -10 to 20 Deg C or broader), Quartz Nebulizer, Ni Sampler, and Skimmer cones. b.The quoted ICP-MS must have the capability to handle TDS greater than or equal to 25% with accessories like UHMI/AMS/AGD 3. Plasma and torch setup a.Computer-controlled 27 to 40MHz or better RF generator operating from 400 to 1600 watts or better for automatic control of torch ignition, shutdown, and system warm-up. b.The Plasma torch should have provision for software-controlled alignment for horizontal position, vertical position, and sampling depth. c.Plasma Gas Control: Consists of at least 3 Mass Flow Controllers (MFC) or equivalent dedicated gas flow controllers with fully computer controlled for control of plasma, auxiliary makeup or Nebulizer 4.Interface a.Standard large orifice Ni sampling cone and skimmer cones of approx. 1.0mm orifice to avoid clogging. b.The system must have 90 Deg deflection mechanisms for removing all neutrals from the Ion path c.The Ion path must be maintenance-free 5.Collision/Reaction Cell a. Cell is capable of operating inall 3 modes- standard, collision and reaction modes. Cell can remove polyatomic interferences as per national and international regulations. Kinetic energy discrimination (KED) /collision facility is available to remove interferences. The reaction cell should allow the use of three gases including Oxygen, Hydrogen, and ammonia in pure form or premix form. b. Cell have provision for fully automated and software-controlled changeover between standard, collision and reaction modes without any manual intervention. c. The cell technology must have a minimum of 2 gas lines -one for pure collision (helium) gas , the second for either oxygen or hydrogen and third for ammonia in pure or premix form. d. Cell must be non-consumable with zero maintenance. System should have Dynamic Bandpass or equivalent with low mass and high mass tuning and extended dynamic range to address wide variety of samples and wide variety of matrices e. The system should have dedicated control devices for Plasma, Auxiliary, Nebulizer, Collision and Reaction gases. In addition a separate controller for handling samples with high TDS. 6. Mass analyser and Detector a.Mass range: 2-280 amu or better. b.Linear Dynamic range: 10 orders of magnitude or better c.Mass scan speed: 3700 amu/s or better d.The ion detector is a simultaneous dual-mode( both analog and digital) discrete dynode electron multiplier, 10 order or more magnitude of dynamic range e.Should be minimum Dwell time of 100 microseconds in both modes f.The dual-mode detector assembly must come standard with the system 7.1 Performance Sensitivity specifications will be considered and document evidences should be provided during demo & installation: a. 7 Li>70 Mcps/mg/l or Kcps/ppb b. 115 In>400Mcps/mg/l or Kcps/ppb c. 238U>300Mcps/mg/l or Kcps/ppb d.Oxide ratio (%) CeO/Ce <2.5 or better e.Ba++ or Ce++/ Ba or Ce <3 or better f.Background noise (no gas mode): <1 cps g.Short Term Stability <2% RSD or better h.Long Term Stability<3% RSD or better i.Isotope-ratio precision: Ag: 0.1% RSD or better 7.2 Detection Limits a. 9Be less than or equal to 0.4 ppt b. 115In less than or equal to 0.1ppt c. 209Bi less than or equal to 0.1 ppt 8. Vacuum system a.Turbo pump should be differential pumping. b.Vacuum can be maintained even in case of a power failure or the system can be backfilled with inert gas or suitable mechanism to prevent damage to collision/reaction cell and quadrupole 9. Software a.Suitable Data Station with all Software controls & future upgrade controls with Instrument software. b.Software should provide comprehensive functionality for analysis through fully automated process with auto tuning. c.Minimum 2 offline software licenses must be supplied as standard. d.Customizability to meet QA/QC functionality needs. e.Automated QA/QC checks 10. Regulatory and Safety Compliance Instrument should comply to- EN 61010-1:2010 and EN 61010-2-081 Safety requirements for Electrical Equipment for Measurement, Control and Laboratory, European EMC Directive 2014/30/EU and referenced standards EN 61326-1:2013, WEEE Directive 2012/19/EU, RoHS 2. 11. Accessories a.Autosampler of minimum sample vial holding capacity of 150 positions or more should be offered. It should be metal free and should have independent X-Y-Z movement.. b.CRM conforming with IS 17034 -Mixed Multielement standard solution (1,000 micro g/mL: Ag, Al, B, Ba, Ca, Cd, Cr, Cu, Fe, K, Li, Mg, Mn, Na, Ni, Pb,As,Hg, Zn) & Single element (100 ppm, 125 ml) standards for Hg & As. c.Minimum PC and Printer requirement: i5 PC, 16GB RAM, 1TB hard drive with 24'' monitor or factory configured PC workstation, along with antivirus, MS office, and ICP-MS software. A compatible multifunction laser printer should be included. d.The offered system should be capable to do speciation in future to couple with LC/IC with more than 50000 or suitable data sets . 12. Additional Requirements 1. All necessary pre-installation requisites/consumables including chemicals, acids, gases and standards for complete installation and demonstration of the instrument should be supplied (details as below). 2. Gas cylinders with regulators (minimum number of cylinders required are mentioned here): 3. Argon - 06 Nos., 4. Helium - 01 Nos., 5. Oxygen- 01 No 6. Hydrogen -01 No 7. 2 Position Argon Gas manifold, Gas Panel. 8. Gas regulators for all gases mentioned -1 each 9. Gas purification panel along with filtering,tubing and all other required accessories. 10. Gas supply manifold for switching gas cylinder 11. Suitable Exhaust System with pump,exhaust pipeline and complete installation 12. A pre installation site visit,assessment is required for site preparation for installation 13. 20 KVA UPS with 30 min backup 14. Compact and low-noise chiller unit(s) as per manufacturer?s recommendation.-1 no 15. Auto-tuning standards. 13. Consumables List -Additional requirement 1) Ni sampler, skimmer cone (05 sets) 2) Standard torch -02 set 3) Standard nebulizer & Spray chamber - 02 Set 4) Standard peristaltic pump tubing for drain (pk/12) - 2 Nos. 5) Standard Peristaltic pump tubing for samples (pk/12) - 2 Nos. 6) Peristaltic pump tubing for ISTD (pk/12) - 2 Nos 7) Tubing autosampler (pk/12) - 2 Nos 8) Graphite gasket for Sampling cone- 5 Nos. 9) Sample tubing for nebulizer 10 Nos. 10) Tubing for spray chamber drain 11) Pump oil (1L) - 3 sets /For the smooth operation of 7 years 12) Skimmer base for Ni cone -05 Set Each 13) Fluid for chiller - 07 L 14) Fluid filter for chiller-2 sets 15) Cone cleaning solvent/supra pure chemical - 02 L 16) Swab (cotton-tipped both ends) - 100 Nos. 17) Autosampler vials - 1000 Nos. 18) Standard autosampler probe and complete tubing set - 01 sets 19) RF Coil/ Lumi Coil-5 sets 20) Torch bonnet-3 sets 14. good quality table (8 feet length* 3 feet width * 2.5 feet height, Anti-vibration table Bottom frame and two side drawers & cabinets made up of powder coated MS of appropriate gauge & strength with thick granite top) should be provided for Installation of Instrument, Computer & Printer.) 15. Warranty Five years warranty from the date of installation on main Instrument, exhaust system, PC-Printer, Chiller, UPS, (Except consumables items) against any kind of manufacturing defects and must include periodic servicing of instrument on-site .AMC should also be quoted beyond warranty period 16. Training 7 Days training on the Instrument at Owner's Site. There will be two training sessions-installation training and after few months an advanced application training. The training should include hardware and software operation, maintenance and trouble shooting.

OD219977/2025-2026:Supply, Installation and commissioning ,testing , training , provision of manpower for operating the instrument and shifting during warranty period of GCMS with all accessories. Specifications: A compact high sensitive GC-MS system along with all accessories as per the specification suitable for the analysis of pesticides residue in water given below with reference to drinking water specification IS 10500:2012 Note: All components of the System may be from the same supplier and amenable to control/data acquisition from the MS software. For third party part, vendor must ensure service support as and when required Technical Specification -GCMS 1).Application requirement The offered system must achieve at least 0.5 times of acceptable limits mentioned as follows Parameters Acceptable limit as per the standard 10500;2012 (Maximum) Parameters concerning toxic substances Pesticide residues i.Alachlor 20µg/l ii.Atrazine 2µg/l iii.Aldrin/ Dieldrin 0.03µg/l iv.Alpha HCH 0.01µg/l v.BetaHCH 0.04µg/l vi.Butachlor 125µg/l vii.Chlorpyriphos 30µg/l viii.DeltaHCH 0.04µg/l ix. DDT (o, p and p, p - Isomers of DDT ,DDE and DDD) 1µg/l x.Endosulfan(alpha, beta,andsulphate) 0.4µg/l xi.Ethion 3µg/l xii.Gamma - HCH (Lindane) 2µg/l xiv. Malathion 190µg/l xv.Methylparathion 0.3µg/l xvi. Monocrotophos 1µg/l xvii.Phorate 2µg/l 2).Gas Chromatograph a.The GC must have all features to provide easy accessibility to the GC and immediate interactions with it, such as carrier gas, column evaluation etc. b Retention Time Repeatability less than or equal to 0.0008 min c Peak area repeatability <0.5 %RSD or better 3).Oven a The column oven should have an operating range from ambient+4°C to 450°C or better b Fast heat-up time-120 °C/min or better c Fast cool-down time 450 °C to 50 °C within 4 minutes or better d The oven temperature stability is within 0.01 °C/ every °C of actual temperature or better f Oven Ramps/Plateaus Cool down. It should have number of ramps/plateaus: 20/21 or better 4).Injector -SSL (2 numbers) and auto sampler a Maximum temperature: 400 °C or better b Split ratio: Up to 12500:1 or better c Pressure range: 0-680 kPa (0-100 psi) or better d Auto sampler should have 15 vial capacity or more 5). Single Quadrupole Mass Spectrometer a Mode (MS) * It should have Full scan, SIM modes should be available 6). Software Features i. It should have Automated acquisition window adjustment based on retention time . It should have a report generation option. 7).Ion Source a It should have EI source or better , with dual filaments,temperature upto 350 °C or better b The instrument should have heated quadrupole to avoid the condensation of sample molecules or equivalent technology should be there . 8).Mass Range a The mass range should be 1.2 to 1050 a.m.u. or better. b Mass axis stability : 0.10 amu/48 hrs or better c Mass resolution -1 amu or better. 9).Scan Rate a The MS should have scan rate up to 20000 a.m.u /second or better 10).Pumping Systems It should have a High capacity( Greater than or equal to 250L/s) turbo molecular pump (TMP) or better 11).Electron Energy *It should have an adjustable electron energy upto 150eV or better 12).Emission Current,dual filaments or better. It should have a emission current of 300 µA or better. 13).Transfer Line Temperature *The Maximum Temperature should be greater than or equal to 350 °C 14).Performance Specifications using octa fluoro naphthalene (OFN) a IDL should be less than or equal to 1.5 fg. Vendor need to demonstrate IDL at the time of installation, so reference specs are not acceptable. 15).Software Features a It should have Automated acquisition window adjustment based on retention time b It should have a software for controlling and acquiring all the GC,MS autosampler. c Report Writer Facility should be available d Latest NIIST Library should be provided e Chromatography data system for control,acquisition, processing,& Reporting software. f Instrument compatible PC and laser should be quoted. 16). Must perform IQ& OQ and PQ of the system on installation to the satisfaction of customer 17). Consumables List (each line items & required Qty should be quoted along with OEM part) (i). Suitable Autosampler syringe - 50 Syringe (ii). Autosampler vials with cap and septa - 500 Nos (iii). Septa for Injector -100 Nos (iv). DB- 5 or equivalent MS column 30m X 0.25 mm X 0.25 - 3 Nos. (v). Filament - 5 nos (vi). GC installation kit - 1 No (vii). Split and splitless Liner - 10 No each (viii). Liner O ring - 20 No (ix). Electron multiplier - 1 No (x).Universal trap for Hydrogen - 2 Nos (xi).Syringe, 25mL Hamilton, cone plunger - 1 No (xii).GCMS tool kit - 1 No (xiii).Test tubes, 25 x 100 mm - 20 Nos 18). CRM standards compliant with ISO 17034 as per Drinking Water Specification IS 10500:2012 given in the list should be provided. 19).Additional Requirements All relevant accessories / consumables (For 50 Nos of sample per month for 5 years need to be quoted separately. * Gas cylinders with regulators (minimum number of cylinders required are mentioned here): * Helium - 04 Nos., * Cylinder Cage to keep 4 cylinders (Cylinder to keep outside the lab) * Required purification panel & Regulator should be offered. * 10 KVA UPS with 60 min Backup * One vibration free bench/table with granite top for keeping complete instrument, PC, autosampler with Dimensions: 9 feet (L) x 3 feet (B) x 3 feet (H) * One- time shifting of instrument and re- installation is to be done (Same campus) 20).Warranty Five (5) years warranty from the date of installation on Main Instrument (with one PM Kit per year), PC-Printer, UPS, Battery,Gas Purification panel, regulator (Except consumables item) 21).Bidder should furnish at least 5 PO copies/performance certificates from the reputed Central/State Govt. & research institutes organizations for similar instrument. 22). Training: 3 training of 5 days each to the user for the mentioned applications must be provided at owner?s site. There will be two training sessions- installation training and after few months an advanced application training. This training include hands on and in depth training on the operation and the maintenance of the system as well a specific application training by application specialist. 23). Manpower One Manpower should be provided for 5 years to operate both GCMS & ICPMS 24).The various components of the system need to be quoted by the same vendor for proper integration ,installation and after sales services