Annual Rate contract for Testing of Milk and Milk Products through External NABL Laboratory at Dudhmansagar Dairy Manesar

MILK & MILK PRODUCTS

S.N. Sample Description Test Parameters Unit Specified Norms Reference Rate (Basic)

1 Poly Pack Pasteurized Milk (Full Cream milk, Toned Milk, Double Tonned milk, Cow Milk, Buffalo Milk) Fat As per variety DGHS : [IS-1224 (Part I) - 1977 Reaffirmed 2003] FSSAI : IS 1479 (Part I) 1961 (Reaffirmed 2003)

Solid Not Fat As per variety

Total Solids%, min As per variety DGHS and FSSAI: IS 12333 -1997 / ISO 6731: 1989 Milk, Cream and Evaporated milk. –Determination of total Solids Content -reference method / Pearsons Composition and Analysis of Foods, 9th edn. Page 570)

Protein As per variety DGHS and FSSAI: A.O.A.C 17th edn, 2000 Official Method 991.23 Protein Nitrogen content of Milk read with 991.20 Nitrogen in Milk- Kjeldahl method and 991.21 Non Protein Nitrogen in Whole Milk

Acidity Max 0.130 % FSSAI: IS 1166 – 1973 Specification for condensed milk. Bureau of Indian Standards, New Delhi

Creaming Index As per variety IS 4238 -1967 (R 2005) (RA 2020)

Ash Contents AOAC 945.46 19th edition: 2012 AOAC 930.30 19 thedition: 2012

pH of Milk 6.6 - 6.8 AOAC Official method 981.12 , ISO 10523:2008 , Pearson's Composition and analysis of Foods, 9th Edition)

Freezing Point of Milk ≤ - 0.525 ◦C FSSAI Milk & Milk Products Regulations , ISO 5764:2009 / IDF 108:2009

Lactose% As per variety AOAC 984.15 / ISO 22662:2007 / IDF 198:2007

Reichert-Meissl Value (extracted fat) min 28 FSSAI : IS 3508 – 1966 (Reaffirmed 1997) Methods of sampling and test for Ghee (Butterfat). Bureau of Indian Standards, New Delhi

BR Test 40 -43 FSSAI: IS 3508 – 1966 (Reaffirmed 1997) Methods of sampling and test for Ghee (Butterfat). Bureau of Indian Standards, New Delhi; Kumar, A.; Lal, D.; Seth, R. and Sharma, R.(2002) Recent trends in detection of adulteration in milk fat: a review: Indian J. Dairy Sci., 55 (6): 319-330. Rangappa, K.S. and Achaya, K.T. 1974. In: Indian Dairy Products. Asia Pub. House, Bombay

Mineral Oil Test Negative DGHS and FSSAI: I.S.I. Handbook of Food Analysis (Part XIII)-1984 Page 89/ A.O.A.C 17th edn, 2000, Official Method 945.102 – Oil (mineral) in fats –Qualitative Test

Animal fats & Vegetable oils/fats (By Valenta and Hager Test) Negative Handbook on Analysis of Milk, Page No. 154

Sugar Test Negative FSSAI: IS 1479 ( Part I) 1961 (Reaffirmed 2003) Methods of test for Dairy Industry – Rapid Examination of Milk. Bureau of Indian Standards, New Delhi

Rosalic Acid Test/ Detection of Neutralizers Negative DGHS & FSSAI: IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi

Starch Test Negative DGHS & FSSAI: I.S.1479 (Part I) – 1960 Methods of test for Dairy Industry, Rapid examination of Milk

Salt Test Negative DGHS & FSSAI: Pearson’s Composition and Analysis of Foods, 9thedn,1991 – Modified Mohr method, page 14

Urea Test (Qualitative ) Negative NDDB, Technews, Nov-Dec 2009,No. 83

Urea Test (Quantitative ) 700 ppm max DGHS : A.O.A.C 17th edn, 2000 Modified Official method 967.07, Urea in animal feed

Nitrates (Pond Water) Test Negative FSSAI: Sharma, R.; Rajput, Y.S. and Naik, N.L. (2012). Detection of adulterants in milk – a laboratory manual. NDRI Publication No. 88/2012, NDRI, Karnal, page 47-48

Sodium Thiosulphate Negative Handbook on Analysis of Milk, Page No. 122

Ammonium Compounds Negative Handbook on Analysis of Milk,Page No. 133

Ammonium Sulphate Negative DGHS & FSSAI: Milk and Milk products Vol. 5 Published by N.C.E.R.T

Cellulose Negative FSSAI: Manual Methods of Analysis for Adulterants & Contaminants in Foods. I.C.M.R 1990

Formalin in Milk Negative DGHS & FSSAI: Method 1:Hehner’s Test: Pearson’s Composition and Analysis of foods, 9th edition, 1991 page 90; IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi

Boric acid and Borates Negative FSSAI: Method 1 & 2: IS 1479 ( Part I) 1961 (Reaffirmed 2003) Methods of test for Dairy Industry – Rapid Examination of Milk. Bureau of Indian Standards, New Delhi

Detection of Hypochlorites Negative DGHS & FSSAI : IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi; A.O.A.C 17th edn, 2000 Official Method 922.08 Hypochlorites and Chloramines in milk

Detection of Maltodextrin Negative FSSAI: IS 1479 (Part II) 1961 (Reaffirmed 1997, being revised) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi.

Detection and Estimation of Added Glucose in Milk Negative DGHS & FSSAI: Manual Methods of Analysis for Adulterants and Contaminants in Foods, I.C.M.R 1990, page 28; Roy, N.K. and Sen, D.C. (1991) Rapid analysis of milk. In: Textbook of Practical Dairy Chemistry. Vol. I. Chemical analysis of fluid milk. Kalyani Publishers, New Delhi, India

Anionic Detergent in Milk Negative FSSAI: Rajput, Y.S.; Sharma, R. and Kaur, S. (2006) A kit for detection of detergent in milk. Indian Patent Office file no. 1970/Del/2006.

Presence of Skimmed milk Powder in Natural milk Absent FSSAI: Journal of Food Science and Technology, Vol 22 (1985) page 207-208

Detection of Gelatine in Milk Absent FSSAI: A.O.A.C 17thedn ,2000 Official Method - 920.106. Gelatine in Milk and Milk products

Presence of Hydrogen Peroxide in Milk Absent FSSAI: Method 1: Vanadium pentoxide Test: A.O.A.C 17thedn, 2000 Official Method 957.08 Hydrogen Peroxide in milk

Salicylic acid in Milk Absent FSSAI: A.O.A.C 17th, edn Official method 975. 30 Salicylic acid in Food and Beverages / IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi).

Melamine 2.5 mg/kg FSSAI: 1. Advisory no.: 2/FSSAI/2008. Advisory to the state health authorities on monitoring melamine contamination of foods. FSSAI, India

Microorganism (As per FSSA, 2006 and Rules & Regulations 2011)

TPC in 1 ml NMT 30,000

Coliform count in 1 ml Less than 10

E. coli in 1 ml Absent

Salmonella in 25 ml Absent

Listeria monocytogens in 25 ml Absent

Aflatoxin M1 , MAX µg/kg 0.5

Melamine mg/kg 2.5 Max

Lead as Pb mg/kg Max 0.02

Copper as Cu mg/kg Max 30

Arsenic as As mg/kg Max 0.1

Tin mg/kg Max 250

Cadmium as Cd mg/kg Max 0.02

Mercury mg/kg Max 1

Methyl Mercury mg/kg Max 0.25

Nickel (Ni) mg/kg Max 0.2

Chromium (Cr) mg/kg Max 1.0

Nutritional Value per 100mL (approx value) As per Declaration

Energy, kcl As per Variety

Saturated Fat, g

Total carbohydrate, g

Insecticides & Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

2,4-Dichlorophenoxy Acetic Acid mg/kg 0.05 Max

Acephate (expressed as mixture of Methamidophos and acephate) mg/kg 0.02 Max

Acetamiprid mg/kg 0.02 Max

Azoxystrobin mg/kg 0.01 Max

Sum of benomyl and carbendazim expressed as carbendazim mg/kg 0.1 Max

Bifenthrin mg/kg 0.2 Max

Bitertanol mg/kg 0.05 Max

Buprofezin mg/kg 0.01 Max

Carbaryl mg/kg 0.05 Max

Carbendazim mg/kg 0.1 Max

Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran) mg/kg 0.05 Max

Chlorantraniliprole mg/kg 0.05 Max

Chlorothalonil mg/kg 0.07 Max

Chlorpyriphos mg/kg 0.02 Max

Chlothianidin (Chlothianidin and its metabolites Thiazolymethylguanidine (TMG), Thiazolymethylurea (TZMU), Methylnitroguanidine (MNG) TMG) mg/kg 0.02 Max

Cypermethrin (sum of isomers) (Fat soluble residue) mg/kg 0.05 Max

Deltamethrin (Decamethrin) mg/kg 0.05 Max

Dichlorvos (DDVP) (content ofdichloroacetaldehyde (D.C.A.) be reported where possible) mg/kg 0.01 Max

Difenoconazole mg/kg 0.02 Max

Dimethoate mg/kg 0.05 Max

Dinotefuran mg/kg 0.1 Max

Mancozeb mg/kg 0.05 Max

Metiram as CS2 mg/kg 0.05 Max

Edifenphos mg/kg 0.01 Max

Emamectin Benzoate mg/kg 0.01 Max

Ethion(Residues to be determined as ethion and its oxygen analogue and expressed as ethion) mg/kg 0.5 Max

Ethofenprox (Etofenprox) mg/kg 0.02 Max

Fenpropathrin mg/kg 0.1 Max

Fenvalerate (Fat soluble residue) mg/kg 0.01 Max

Fipronil mg/kg 0.02 Max

Flubendiamide mg/kg 0.1 Max

Flusilazole mg/kg 0.05 Max

Glufosinate Ammonium mg/kg 0.02 Max

Imidacloprid mg/kg 0.1 Max

Indoxacarb mg/kg 0.1 Max

Kresoxim Methyl mg/kg 0.01 Max

Methomyl mg/kg 0.02 Max

Methyl Chlorophenoxy Acetic Acid (MCPA) mg/kg 0.04 Max

Metolachlor mg/kg 0.01 Max

Monocrotophos mg/kg 0.02 Max

Oxydemeton-Methyl mg/kg 0.01 Max

Paraquat dichloride (Determined as Paraquatcations) mg/kg 0.01 Max

Penconazole mg/kg 0.01 Max

Phenthoate mg/kg 0.01 Max

Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate) mg/kg 0.05 Max

Pirimiphos-methyl mg/kg 0.05 Max

Propiconazole mg/kg 0.01 Max

Pyraclostrobin mg/kg 0.03 Max

Tebuconazole mg/kg 0.01 Max

Thiacloprid mg/kg 0.05 Max

Thiamethoxam mg/kg 0.05 Max

Thiophanate-Methyl mg/kg 0.05 Max

Trichlorfon mg/kg 0.05 Max

Triacontanol mg/kg 0.01 Max

Triadimefon mg/kg 0.01 Max

Banned Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

Aldicarb mg/kg ND

Aldrin mg/kg ND

Dieldrin mg/kg ND

Chlordane mg/kg ND

Heptachlor mg/kg ND

Lindane (Gamma-HCH) mg/kg ND

Endosulfan mg/kg ND

Phosphamidon mg/kg ND

Captafol mg/kg ND

Formothion mg/kg ND

Simazine mg/kg ND

Diazinon mg/kg ND

2,4 DDT mg/kg ND

4,4 DDT mg/kg ND

2,4 DDD mg/kg ND

4,4 DDD mg/kg ND

2,4 DDE mg/kg ND

4,4 DDE mg/kg ND

Fenitrothion mg/kg ND

Fenthion mg/kg ND

Methyl Parathion mg/kg ND

Ethyl Parathion mg/kg ND

Ferbam as CS2 mg/kg ND

Antibiotics (As per FSSA, 2006 and Rules & Regulations 2011)

Ampicillin mg/kg 0.01 Max

Chlortetracycline mg/kg 0.1 Max

Oxytetracycline mg/kg 0.1 Max

Tetracycline mg/kg 0.1 Max

Lincomycin mg/kg 0.15 Max

Neomycin mg/kg 1.5 Max

Spectinomycin mg/l 0.2 Max

Trimethoprim mg/kg 0.01 Max

Sulfadiazine mg/kg 0.01 Max

Sulfanilamide mg/kg 0.01 Max

Apramycin mg/kg 0.01 Max

Ceftiofur, mg/l mg/l 0.1 Max

Monensi mg/kg 0.002 Max

Sulphaquinoxaline mg/kg 0.01 Max

Sulfadimidine mg/kg 0.025 Max

Tylosin mg/kg 0.1 Max

Virginiamycin mg/kg 0.01 Max

Albendazole mg/kg 0.1 Max

Doramectin mg/kg 0.015 Max

Flunixin mg/kg 0.01 Max

Ivermectin mg/kg 0.01 Max

Meloxicam mg/kg 0.01 Max

Febantel mg/kg 0.1 Max

Fenbendazole mg/kg 0.1 Max

Oxyfendazole mg/kg 0.1 Max

Oxyclozanide mg/kg 0.01 Max

Sulphachloropyrazine mg/kg 0.01 Max

Parbendazole mg/kg 0.01 Max

Praziquantel mg/kg 0.01 Max

Thiabendazole mg/kg 0.1 Max

Diminazene mg/kg 0.15 Max

Cefphactril mg/kg 0.01 Max

BANNED ANTIBIOTICS (As per FSSA, 2006 and Rules & Regulations 2011)

Carbadox mg/kg ND

Chloramphenicol mg/kg ND

Chlorpromazine mg/kg ND

Clenbuterol mg/kg ND

Colistin mg/kg ND

Crystal Violet (Sum of Crystal Violet and Leucocrystal Violet) mg/kg ND

Glycopeptides mg/kg ND

Malachite Green (Sum of Malachite green and Leucomalachite green) mg/kg ND

Nitrofurans and its metabolites furazolidone (AOZ), nitrofurazone (SEM), furaltadone (AMOZ) and nitrofurantoin (AHD) mg/kg ND

Streptomycin and its metabolite dihydrostreptomycin mg/kg ND

Nitroimidazoles including- mg/kg ND

Dimetridazole (DMZ) mg/kg ND

Ronidazole (RNZ) and its metabolite 2-hydroxymethyl-1-methyl-3 nitroimidazole(HMMNI) mg/kg ND

Ipronidazole (IPZ) and its metabolite Hydroxyipronidazole mg/kg ND

Metronidazole (MNZ) and its metabolite 3 hydroxymetronidazole mg/kg ND

Steroids mg/kg ND

Stilbenes mg/kg ND

Sulphamethoxazole mg/kg ND

2 UHT tonned/DTM milk (Amul Moti UHT Treated Homogenized Tonned/DTM Milk) Fat As per variety DGHS : [IS-1224 (Part I) - 1977 Reaffirmed 2003] FSSAI : IS 1479 (Part I) 1961 (Reaffirmed 2003)

Solid Not Fat As per variety

Total Solids%, min As per variety DGHS and FSSAI: IS 12333 -1997 / ISO 6731: 1989 Milk, Cream and Evaporated milk. –Determination of total Solids Content -reference method / Pearsons Composition and Analysis of Foods, 9th edn. Page 570)

Protein As per variety DGHS and FSSAI: A.O.A.C 17th edn, 2000 Official Method 991.23 Protein Nitrogen content of Milk read with 991.20 Nitrogen in Milk- Kjeldahl method and 991.21 Non Protein Nitrogen in Whole Milk

Acidity Max 0.130 % FSSAI: IS 1166 – 1973 Specification for condensed milk. Bureau of Indian Standards, New Delhi

Creaming Index As per variety IS 4238 -1967 (R 2005) (RA 2020)

Ash Contents AOAC 945.46 19th edition: 2012 AOAC 930.30 19 thedition: 2012

Lactose% As per variety AOAC 984.15 / ISO 22662:2007 / IDF 198:2007

Reichert-Meissl Value (extracted fat) min 28 FSSAI : IS 3508 – 1966 (Reaffirmed 1997) Methods of sampling and test for Ghee (Butterfat). Bureau of Indian Standards, New Delhi

BR Test 40 -43 FSSAI: IS 3508 – 1966 (Reaffirmed 1997) Methods of sampling and test for Ghee (Butterfat). Bureau of Indian Standards, New Delhi; Kumar, A.; Lal, D.; Seth, R. and Sharma, R.(2002) Recent trends in detection of adulteration in milk fat: a review: Indian J. Dairy Sci., 55 (6): 319-330. Rangappa, K.S. and Achaya, K.T. 1974. In: Indian Dairy Products. Asia Pub. House, Bombay

Mineral Oil Test Negative DGHS and FSSAI: I.S.I. Handbook of Food Analysis (Part XIII)-1984 Page 89/ A.O.A.C 17th edn, 2000, Official Method 945.102 – Oil (mineral) in fats –Qualitative Test

Animal fats & Vegetable oils/fats (By Valenta and Hager Test) Negative Handbook on Analysis of Milk, Page No. 154

Sugar Test Negative FSSAI: IS 1479 ( Part I) 1961 (Reaffirmed 2003) Methods of test for Dairy Industry – Rapid Examination of Milk. Bureau of Indian Standards, New Delhi

Rosalic Acid Test/ Detection of Neutralizers Negative DGHS & FSSAI: IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi

Starch Test Negative DGHS & FSSAI: I.S.1479 (Part I) – 1960 Methods of test for Dairy Industry, Rapid examination of Milk

Salt Test Negative DGHS & FSSAI: Pearson’s Composition and Analysis of Foods, 9thedn,1991 – Modified Mohr method, page 14

Urea Test (Qualitative ) Negative NDDB, Technews, Nov-Dec 2009,No. 83

Urea Test (Quantitative ) 700 ppm max DGHS : A.O.A.C 17th edn, 2000 Modified Official method 967.07, Urea in animal feed

Nitrates (Pond Water) Test Negative FSSAI: Sharma, R.; Rajput, Y.S. and Naik, N.L. (2012). Detection of adulterants in milk – a laboratory manual. NDRI Publication No. 88/2012, NDRI, Karnal, page 47-48

Sodium Thiosulphate Negative Handbook on Analysis of Milk, Page No. 122

Ammonium Compounds Negative Handbook on Analysis of Milk,Page No. 133

Ammonium Sulphate Negative DGHS & FSSAI: Milk and Milk products Vol. 5 Published by N.C.E.R.T

Cellulose Negative FSSAI: Manual Methods of Analysis for Adulterants & Contaminants in Foods. I.C.M.R 1990

Formalin in Milk Negative DGHS & FSSAI: Method 1:Hehner’s Test: Pearson’s Composition and Analysis of foods, 9th edition, 1991 page 90; IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi

Boric acid and Borates Negative FSSAI: Method 1 & 2: IS 1479 ( Part I) 1961 (Reaffirmed 2003) Methods of test for Dairy Industry – Rapid Examination of Milk. Bureau of Indian Standards, New Delhi

Detection of Hypochlorites Negative DGHS & FSSAI : IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi; A.O.A.C 17th edn, 2000 Official Method 922.08 Hypochlorites and Chloramines in milk

Detection of Maltodextrin Negative FSSAI: IS 1479 (Part II) 1961 (Reaffirmed 1997, being revised) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi.

Detection and Estimation of Added Glucose in Milk Negative DGHS & FSSAI: Manual Methods of Analysis for Adulterants and Contaminants in Foods, I.C.M.R 1990, page 28; Roy, N.K. and Sen, D.C. (1991) Rapid analysis of milk. In: Textbook of Practical Dairy Chemistry. Vol. I. Chemical analysis of fluid milk. Kalyani Publishers, New Delhi, India

Anionic Detergent in Milk Negative FSSAI: Rajput, Y.S.; Sharma, R. and Kaur, S. (2006) A kit for detection of detergent in milk. Indian Patent Office file no. 1970/Del/2006.

Presence of Skimmed milk Powder in Natural milk Absent FSSAI: Journal of Food Science and Technology, Vol 22 (1985) page 207-208

Detection of Gelatine in Milk Absent FSSAI: A.O.A.C 17thedn ,2000 Official Method - 920.106. Gelatine in Milk and Milk products

Presence of Hydrogen Peroxide in Milk Absent FSSAI: Method 1: Vanadium pentoxide Test: A.O.A.C 17thedn, 2000 Official Method 957.08 Hydrogen Peroxide in milk

Salicylic acid in Milk Absent FSSAI: A.O.A.C 17th, edn Official method 975. 30 Salicylic acid in Food and Beverages / IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi).

Turbidity test To confirm to test IS 4238 -1967 (R 2005) (RA 2020)

pH variation on 7 days of incubation 0.3 max IS 4238 -1967 (R 2005) (RA 2020)

Titrable acidity variation on 7 days of incubation 0.02 max IS 4238 -1967 (R 2005) (RA 2020)

Microorganism (As per FSSA, 2006 and Rules & Regulations 2011)

Aerobic (B. cereus) in 1 ml Nil

Anaerobic (Clostridium Perfringern) in 1 ml Nil

Coliform count in 1 ml -

E. coli in 1 ml -

Shigella in 25 ml -

Salmonella in 25 ml -

S. aureus in 1 ml -

Yeast and Mould in 1 ml -

Listeria monocytogens in 1 ml -

Bacterial spores in 1 ml Max 5

Aflatoxin M1 , MAX µg/kg 0.5

Melamine mg/kg 2.5 Max

Lead as Pb mg/kg Max 0.02

Copper as Cu mg/kg Max 30

Arsenic as As mg/kg Max 0.1

Tin mg/kg Max 250

Cadmium as Cd mg/kg Max 0.02

Mercury mg/kg Max 1

Methyl Mercury mg/kg Max 0.25

Nickel (Ni) mg/kg Max 0.2

Chromium (Cr) mg/kg Max 1.0

Nutritional Value per 100mL (approx value) As per Declaration

Energy, kcl As per Variety

Saturated Fat, g

Total carbohydrate, g

Insecticides & Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

2,4-Dichlorophenoxy Acetic Acid mg/kg 0.05 Max

Acephate (expressed as mixture of Methamidophos and acephate) mg/kg 0.02 Max

Acetamiprid mg/kg 0.02 Max

Azoxystrobin mg/kg 0.01 Max

Sum of benomyl and carbendazim expressed as carbendazim mg/kg 0.1 Max

Bifenthrin mg/kg 0.2 Max

Bitertanol mg/kg 0.05 Max

Buprofezin mg/kg 0.01 Max

Carbaryl mg/kg 0.05 Max

Carbendazim mg/kg 0.1 Max

Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran) mg/kg 0.05 Max

Chlorantraniliprole mg/kg 0.05 Max

Chlorothalonil mg/kg 0.07 Max

Chlorpyriphos mg/kg 0.02 Max

Chlothianidin (Chlothianidin and its metabolites Thiazolymethylguanidine (TMG), Thiazolymethylurea (TZMU), Methylnitroguanidine (MNG) TMG) mg/kg 0.02 Max

Cypermethrin (sum of isomers) (Fat soluble residue) mg/kg 0.05 Max

Deltamethrin (Decamethrin) mg/kg 0.05 Max

Dichlorvos (DDVP) (content ofdichloroacetaldehyde (D.C.A.) be reported where possible) mg/kg 0.01 Max

Difenoconazole mg/kg 0.02 Max

Dimethoate mg/kg 0.05 Max

Dinotefuran mg/kg 0.1 Max

Mancozeb mg/kg 0.05 Max

Metiram as CS2 mg/kg 0.05 Max

Edifenphos mg/kg 0.01 Max

Emamectin Benzoate mg/kg 0.01 Max

Ethion(Residues to be determined as ethion and its oxygen analogue and expressed as ethion) mg/kg 0.5 Max

Ethofenprox (Etofenprox) mg/kg 0.02 Max

Fenpropathrin mg/kg 0.1 Max

Fenvalerate (Fat soluble residue) mg/kg 0.01 Max

Fipronil mg/kg 0.02 Max

Flubendiamide mg/kg 0.1 Max

Flusilazole mg/kg 0.05 Max

Glufosinate Ammonium mg/kg 0.02 Max

Imidacloprid mg/kg 0.1 Max

Indoxacarb mg/kg 0.1 Max

Kresoxim Methyl mg/kg 0.01 Max

Methomyl mg/kg 0.02 Max

Methyl Chlorophenoxy Acetic Acid (MCPA) mg/kg 0.04 Max

Metolachlor mg/kg 0.01 Max

Monocrotophos mg/kg 0.02 Max

Oxydemeton-Methyl mg/kg 0.01 Max

Paraquat dichloride (Determined as Paraquatcations) mg/kg 0.01 Max

Penconazole mg/kg 0.01 Max

Phenthoate mg/kg 0.01 Max

Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate) mg/kg 0.05 Max

Pirimiphos-methyl mg/kg 0.05 Max

Propiconazole mg/kg 0.01 Max

Pyraclostrobin mg/kg 0.03 Max

Tebuconazole mg/kg 0.01 Max

Thiacloprid mg/kg 0.05 Max

Thiamethoxam mg/kg 0.05 Max

Thiophanate-Methyl mg/kg 0.05 Max

Trichlorfon mg/kg 0.05 Max

Triacontanol mg/kg 0.01 Max

Triadimefon mg/kg 0.01 Max

Banned Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

Aldicarb mg/kg ND

Aldrin mg/kg ND

Dieldrin mg/kg ND

Chlordane mg/kg ND

Heptachlor mg/kg ND

Lindane (Gamma-HCH) mg/kg ND

Endosulfan mg/kg ND

Phosphamidon mg/kg ND

Captafol mg/kg ND

Formothion mg/kg ND

Simazine mg/kg ND

Diazinon mg/kg ND

2,4 DDT mg/kg ND

4,4 DDT mg/kg ND

2,4 DDD mg/kg ND

4,4 DDD mg/kg ND

2,4 DDE mg/kg ND

4,4 DDE mg/kg ND

Fenitrothion mg/kg ND

Fenthion mg/kg ND

Methyl Parathion mg/kg ND

Ethyl Parathion mg/kg ND

Ferbam as CS2 mg/kg ND

Antibiotics (As per FSSA, 2006 and Rules & Regulations 2011)

Ampicillin mg/kg 0.01 Max

Chlortetracycline mg/kg 0.1 Max

Oxytetracycline mg/kg 0.1 Max

Tetracycline mg/kg 0.1 Max

Lincomycin mg/kg 0.15 Max

Neomycin mg/kg 1.5 Max

Spectinomycin mg/l 0.2 Max

Trimethoprim mg/kg 0.01 Max

Sulfadiazine mg/kg 0.01 Max

Sulfanilamide mg/kg 0.01 Max

Apramycin mg/kg 0.01 Max

Ceftiofur, mg/l mg/l 0.1 Max

Monensi mg/kg 0.002 Max

Sulphaquinoxaline mg/kg 0.01 Max

Sulfadimidine mg/kg 0.025 Max

Tylosin mg/kg 0.1 Max

Virginiamycin mg/kg 0.01 Max

Albendazole mg/kg 0.1 Max

Doramectin mg/kg 0.015 Max

Flunixin mg/kg 0.01 Max

Ivermectin mg/kg 0.01 Max

Meloxicam mg/kg 0.01 Max

Febantel mg/kg 0.1 Max

Fenbendazole mg/kg 0.1 Max

Oxyfendazole mg/kg 0.1 Max

Oxyclozanide mg/kg 0.01 Max

Sulphachloropyrazine mg/kg 0.01 Max

Parbendazole mg/kg 0.01 Max

Praziquantel mg/kg 0.01 Max

Thiabendazole mg/kg 0.1 Max

Diminazene mg/kg 0.15 Max

Cefphactril mg/kg 0.01 Max

BANNED ANTIBIOTICS (As per FSSA, 2006 and Rules & Regulations 2011)

Carbadox mg/kg ND

Chloramphenicol mg/kg ND

Chlorpromazine mg/kg ND

Clenbuterol mg/kg ND

Colistin mg/kg ND

Crystal Violet (Sum of Crystal Violet and Leucocrystal Violet) mg/kg ND

Glycopeptides mg/kg ND

Malachite Green (Sum of Malachite green and Leucomalachite green) mg/kg ND

Nitrofurans and its metabolites furazolidone (AOZ), nitrofurazone (SEM), furaltadone (AMOZ) and nitrofurantoin (AHD) mg/kg ND

Streptomycin and its metabolite dihydrostreptomycin mg/kg ND

Nitroimidazoles including- mg/kg ND

Dimetridazole (DMZ) mg/kg ND

Ronidazole (RNZ) and its metabolite 2-hydroxymethyl-1-methyl-3 nitroimidazole(HMMNI) mg/kg ND

Ipronidazole (IPZ) and its metabolite Hydroxyipronidazole mg/kg ND

Metronidazole (MNZ) and its metabolite 3 hydroxymetronidazole mg/kg ND

Steroids mg/kg ND

Stilbenes mg/kg ND

Sulphamethoxazole mg/kg ND

3 Amul Probiotic Buttermilk Fat As per variety DGHS : [IS-1224 (Part I) - 1977 Reaffirmed 2003] FSSAI : IS 1479 (Part I) 1961 (Reaffirmed 2003)

Solid Not Fat As per variety

Total Solids%, min As per variety DGHS and FSSAI: IS 12333 -1997 / ISO 6731: 1989 Milk, Cream and Evaporated milk. –Determination of total Solids Content -reference method / Pearsons Composition and Analysis of Foods, 9th edn. Page 570)

Protein As per variety DGHS and FSSAI: A.O.A.C 17th edn, 2000 Official Method 991.23 Protein Nitrogen content of Milk read with 991.20 Nitrogen in Milk- Kjeldahl method and 991.21 Non Protein Nitrogen in Whole Milk

Acidity Max 0.130 % FSSAI: IS 1166 – 1973 Specification for condensed milk. Bureau of Indian Standards, New Delhi

Ash Contents AOAC 945.46 19th edition: 2012 AOAC 930.30 19 thedition: 2012

Microorganism (As per FSSA, 2006 and Rules & Regulations 2011)

Probiotic count per serving

Coliform count in 1 gm NMT 10

E. coli in 1 gm Absent

Salmonella in 25gm Absent

Shigella in 25gm Absent

S. aureus in 1 gm NMT 10

Yeast and Mould in 1 gm NMT 50

Listeria monocytogens in 1 gm Absent

Total Aflatoxin µg/kg 15

Melamine mg/kg 2.5 Max

Lead as Pb mg/kg Max 0.02

Copper as Cu mg/kg Max 30

Arsenic as As mg/kg Max 0.1

Tin mg/kg Max 250

Cadmium as Cd mg/kg Max 0.02

Mercury mg/kg Max 1

Methyl Mercury mg/kg Max 0.25

Nickel (Ni) mg/kg Max 0.2

Chromium (Cr) mg/kg Max 1.0

Nutritional Value per 100mL (approx value) As per Declaration

Energy, kcl As per Variety

Saturated Fat, g

Total carbohydrate, g

Insecticides & Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

2,4-Dichlorophenoxy Acetic Acid mg/kg 0.05 Max

Acephate (expressed as mixture of Methamidophos and acephate) mg/kg 0.02 Max

Acetamiprid mg/kg 0.02 Max

Azoxystrobin mg/kg 0.01 Max

Sum of benomyl and carbendazim expressed as carbendazim mg/kg 0.1 Max

Bifenthrin mg/kg 0.2 Max

Bitertanol mg/kg 0.05 Max

Buprofezin mg/kg 0.01 Max

Carbaryl mg/kg 0.05 Max

Carbendazim mg/kg 0.1 Max

Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran) mg/kg 0.05 Max

Chlorantraniliprole mg/kg 0.05 Max

Chlorothalonil mg/kg 0.07 Max

Chlorpyriphos mg/kg 0.02 Max

Chlothianidin (Chlothianidin and its metabolites Thiazolymethylguanidine (TMG), Thiazolymethylurea (TZMU), Methylnitroguanidine (MNG) TMG) mg/kg 0.02 Max

Cypermethrin (sum of isomers) (Fat soluble residue) mg/kg 0.05 Max

Deltamethrin (Decamethrin) mg/kg 0.05 Max

Dichlorvos (DDVP) (content ofdichloroacetaldehyde (D.C.A.) be reported where possible) mg/kg 0.01 Max

Difenoconazole mg/kg 0.02 Max

Dimethoate mg/kg 0.05 Max

Dinotefuran mg/kg 0.1 Max

Mancozeb mg/kg 0.05 Max

Metiram as CS2 mg/kg 0.05 Max

Edifenphos mg/kg 0.01 Max

Emamectin Benzoate mg/kg 0.01 Max

Ethion(Residues to be determined as ethion and its oxygen analogue and expressed as ethion) mg/kg 0.5 Max

Ethofenprox (Etofenprox) mg/kg 0.02 Max

Fenpropathrin mg/kg 0.1 Max

Fenvalerate (Fat soluble residue) mg/kg 0.01 Max

Fipronil mg/kg 0.02 Max

Flubendiamide mg/kg 0.1 Max

Flusilazole mg/kg 0.05 Max

Glufosinate Ammonium mg/kg 0.02 Max

Imidacloprid mg/kg 0.1 Max

Indoxacarb mg/kg 0.1 Max

Kresoxim Methyl mg/kg 0.01 Max

Methomyl mg/kg 0.02 Max

Methyl Chlorophenoxy Acetic Acid (MCPA) mg/kg 0.04 Max

Metolachlor mg/kg 0.01 Max

Monocrotophos mg/kg 0.02 Max

Oxydemeton-Methyl mg/kg 0.01 Max

Paraquat dichloride (Determined as Paraquatcations) mg/kg 0.01 Max

Penconazole mg/kg 0.01 Max

Phenthoate mg/kg 0.01 Max

Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate) mg/kg 0.05 Max

Pirimiphos-methyl mg/kg 0.05 Max

Propiconazole mg/kg 0.01 Max

Pyraclostrobin mg/kg 0.03 Max

Tebuconazole mg/kg 0.01 Max

Thiacloprid mg/kg 0.05 Max

Thiamethoxam mg/kg 0.05 Max

Thiophanate-Methyl mg/kg 0.05 Max

Trichlorfon mg/kg 0.05 Max

Triacontanol mg/kg 0.01 Max

Triadimefon mg/kg 0.01 Max

Banned Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

Aldicarb mg/kg ND

Aldrin mg/kg ND

Dieldrin mg/kg ND

Chlordane mg/kg ND

Heptachlor mg/kg ND

Lindane (Gamma-HCH) mg/kg ND

Endosulfan mg/kg ND

Phosphamidon mg/kg ND

Captafol mg/kg ND

Formothion mg/kg ND

Simazine mg/kg ND

Diazinon mg/kg ND

2,4 DDT mg/kg ND

4,4 DDT mg/kg ND

2,4 DDD mg/kg ND

4,4 DDD mg/kg ND

2,4 DDE mg/kg ND

4,4 DDE mg/kg ND

Fenitrothion mg/kg ND

Fenthion mg/kg ND

Methyl Parathion mg/kg ND

Ethyl Parathion mg/kg ND

Ferbam as CS2 mg/kg ND

Antibiotics (As per FSSA, 2006 and Rules & Regulations 2011)

Ampicillin mg/kg 0.01 Max

Chlortetracycline mg/kg 0.1 Max

Oxytetracycline mg/kg 0.1 Max

Tetracycline mg/kg 0.1 Max

Lincomycin mg/kg 0.15 Max

Neomycin mg/kg 1.5 Max

Spectinomycin mg/l 0.2 Max

Trimethoprim mg/kg 0.01 Max

Sulfadiazine mg/kg 0.01 Max

Sulfanilamide mg/kg 0.01 Max

Apramycin mg/kg 0.01 Max

Ceftiofur, mg/l mg/l 0.1 Max

Monensi mg/kg 0.002 Max

Sulphaquinoxaline mg/kg 0.01 Max

Sulfadimidine mg/kg 0.025 Max

Tylosin mg/kg 0.1 Max

Virginiamycin mg/kg 0.01 Max

Albendazole mg/kg 0.1 Max

Doramectin mg/kg 0.015 Max

Flunixin mg/kg 0.01 Max

Ivermectin mg/kg 0.01 Max

Meloxicam mg/kg 0.01 Max

Febantel mg/kg 0.1 Max

Fenbendazole mg/kg 0.1 Max

Oxyfendazole mg/kg 0.1 Max

Oxyclozanide mg/kg 0.01 Max

Sulphachloropyrazine mg/kg 0.01 Max

Parbendazole mg/kg 0.01 Max

Praziquantel mg/kg 0.01 Max

Thiabendazole mg/kg 0.1 Max

Diminazene mg/kg 0.15 Max

Cefphactril mg/kg 0.01 Max

BANNED ANTIBIOTICS (As per FSSA, 2006 and Rules & Regulations 2011)

Carbadox mg/kg ND

Chloramphenicol mg/kg ND

Chlorpromazine mg/kg ND

Clenbuterol mg/kg ND

Colistin mg/kg ND

Crystal Violet (Sum of Crystal Violet and Leucocrystal Violet) mg/kg ND

Glycopeptides mg/kg ND

Malachite Green (Sum of Malachite green and Leucomalachite green) mg/kg ND

Nitrofurans and its metabolites furazolidone (AOZ), nitrofurazone (SEM), furaltadone (AMOZ) and nitrofurantoin (AHD) mg/kg ND

Streptomycin and its metabolite dihydrostreptomycin mg/kg ND

Nitroimidazoles including- mg/kg ND

Dimetridazole (DMZ) mg/kg ND

Ronidazole (RNZ) and its metabolite 2-hydroxymethyl-1-methyl-3 nitroimidazole(HMMNI) mg/kg ND

Ipronidazole (IPZ) and its metabolite Hydroxyipronidazole mg/kg ND

Metronidazole (MNZ) and its metabolite 3 hydroxymetronidazole mg/kg ND

Steroids mg/kg ND

Stilbenes mg/kg ND

Sulphamethoxazole mg/kg ND

4 Amul Dahi (Lite/Masti/Premium/ Buffalo/High Protein/Tonned ) Fat As per variety DGHS : [IS-1224 (Part I) - 1977 Reaffirmed 2003] FSSAI : IS 1479 (Part I) 1961 (Reaffirmed 2003)

Solid Not Fat As per variety

Total Solids%, min As per variety DGHS and FSSAI: IS 12333 -1997 / ISO 6731: 1989 Milk, Cream and Evaporated milk. –Determination of total Solids Content -reference method / Pearsons Composition and Analysis of Foods, 9th edn. Page 570)

Protein As per variety DGHS and FSSAI: A.O.A.C 17th edn, 2000 Official Method 991.23 Protein Nitrogen content of Milk read with 991.20 Nitrogen in Milk- Kjeldahl method and 991.21 Non Protein Nitrogen in Whole Milk

Acidity As per variety FSSAI: IS 1166 – 1973 Specification for condensed milk. Bureau of Indian Standards, New Delhi

Ash Contents AOAC 945.46 19th edition: 2012 AOAC 930.30 19 thedition: 2012

Lactose Residue Max 0.1 (For High proten Dahi only) AOAC 945.46 19th edition: 2012 AOAC 930.30 19 thedition: 2012

Microorganism (As per FSSA, 2006 and Rules & Regulations 2011)

Starter Bacteria (min.) in 1 gm

Coliform count in 1 gm NMT 10

E. coli in 1 gm Absent

Shigella in 25gm Absent

Salmonella in 25gm Absent

S. aureus in 1 gm NMT 10

Yeast and Mould in 1 gm NMT 50

Listeria monocytogens in 1 gm Absent

Total Aflatoxin µg/kg 15

Melamine mg/kg 2.5 Max

Lead as Pb mg/kg Max 0.02

Copper as Cu mg/kg Max 30

Arsenic as As mg/kg Max 0.1

Tin mg/kg Max 250

Cadmium as Cd mg/kg Max 0.02

Mercury mg/kg Max 1

Methyl Mercury mg/kg Max 0.25

Nickel (Ni) mg/kg Max 0.2

Chromium (Cr) mg/kg Max 1.0

Nutritional Value per 100mL (approx value) As per Declaration

Energy, kcl As per Variety

Saturated Fat, g

Total carbohydrate, g

Insecticides & Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

2,4-Dichlorophenoxy Acetic Acid mg/kg 0.05 Max

Acephate (expressed as mixture of Methamidophos and acephate) mg/kg 0.02 Max

Acetamiprid mg/kg 0.02 Max

Azoxystrobin mg/kg 0.01 Max

Sum of benomyl and carbendazim expressed as carbendazim mg/kg 0.1 Max

Bifenthrin mg/kg 0.2 Max

Bitertanol mg/kg 0.05 Max

Buprofezin mg/kg 0.01 Max

Carbaryl mg/kg 0.05 Max

Carbendazim mg/kg 0.1 Max

Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran) mg/kg 0.05 Max

Chlorantraniliprole mg/kg 0.05 Max

Chlorothalonil mg/kg 0.07 Max

Chlorpyriphos mg/kg 0.02 Max

Chlothianidin (Chlothianidin and its metabolites Thiazolymethylguanidine (TMG), Thiazolymethylurea (TZMU), Methylnitroguanidine (MNG) TMG) mg/kg 0.02 Max

Cypermethrin (sum of isomers) (Fat soluble residue) mg/kg 0.05 Max

Deltamethrin (Decamethrin) mg/kg 0.05 Max

Dichlorvos (DDVP) (content ofdichloroacetaldehyde (D.C.A.) be reported where possible) mg/kg 0.01 Max

Difenoconazole mg/kg 0.02 Max

Dimethoate mg/kg 0.05 Max

Dinotefuran mg/kg 0.1 Max

Mancozeb mg/kg 0.05 Max

Metiram as CS2 mg/kg 0.05 Max

Edifenphos mg/kg 0.01 Max

Emamectin Benzoate mg/kg 0.01 Max

Ethion(Residues to be determined as ethion and its oxygen analogue and expressed as ethion) mg/kg 0.5 Max

Ethofenprox (Etofenprox) mg/kg 0.02 Max

Fenpropathrin mg/kg 0.1 Max

Fenvalerate (Fat soluble residue) mg/kg 0.01 Max

Fipronil mg/kg 0.02 Max

Flubendiamide mg/kg 0.1 Max

Flusilazole mg/kg 0.05 Max

Glufosinate Ammonium mg/kg 0.02 Max

Imidacloprid mg/kg 0.1 Max

Indoxacarb mg/kg 0.1 Max

Kresoxim Methyl mg/kg 0.01 Max

Methomyl mg/kg 0.02 Max

Methyl Chlorophenoxy Acetic Acid (MCPA) mg/kg 0.04 Max

Metolachlor mg/kg 0.01 Max

Monocrotophos mg/kg 0.02 Max

Oxydemeton-Methyl mg/kg 0.01 Max

Paraquat dichloride (Determined as Paraquatcations) mg/kg 0.01 Max

Penconazole mg/kg 0.01 Max

Phenthoate mg/kg 0.01 Max

Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate) mg/kg 0.05 Max

Pirimiphos-methyl mg/kg 0.05 Max

Propiconazole mg/kg 0.01 Max

Pyraclostrobin mg/kg 0.03 Max

Tebuconazole mg/kg 0.01 Max

Thiacloprid mg/kg 0.05 Max

Thiamethoxam mg/kg 0.05 Max

Thiophanate-Methyl mg/kg 0.05 Max

Trichlorfon mg/kg 0.05 Max

Triacontanol mg/kg 0.01 Max

Triadimefon mg/kg 0.01 Max

Banned Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

Aldicarb mg/kg ND

Aldrin mg/kg ND

Dieldrin mg/kg ND

Chlordane mg/kg ND

Heptachlor mg/kg ND

Lindane (Gamma-HCH) mg/kg ND

Endosulfan mg/kg ND

Phosphamidon mg/kg ND

Captafol mg/kg ND

Formothion mg/kg ND

Simazine mg/kg ND

Diazinon mg/kg ND

2,4 DDT mg/kg ND

4,4 DDT mg/kg ND

2,4 DDD mg/kg ND

4,4 DDD mg/kg ND

2,4 DDE mg/kg ND

4,4 DDE mg/kg ND

Fenitrothion mg/kg ND

Fenthion mg/kg ND

Methyl Parathion mg/kg ND

Ethyl Parathion mg/kg ND

Ferbam as CS2 mg/kg ND

Antibiotics (As per FSSA, 2006 and Rules & Regulations 2011)

Ampicillin mg/kg 0.01 Max

Chlortetracycline mg/kg 0.1 Max

Oxytetracycline mg/kg 0.1 Max

Tetracycline mg/kg 0.1 Max

Lincomycin mg/kg 0.15 Max

Neomycin mg/kg 1.5 Max

Spectinomycin mg/l 0.2 Max

Trimethoprim mg/kg 0.01 Max

Sulfadiazine mg/kg 0.01 Max

Sulfanilamide mg/kg 0.01 Max

Apramycin mg/kg 0.01 Max

Ceftiofur, mg/l mg/l 0.1 Max

Monensi mg/kg 0.002 Max

Sulphaquinoxaline mg/kg 0.01 Max

Sulfadimidine mg/kg 0.025 Max

Tylosin mg/kg 0.1 Max

Virginiamycin mg/kg 0.01 Max

Albendazole mg/kg 0.1 Max

Doramectin mg/kg 0.015 Max

Flunixin mg/kg 0.01 Max

Ivermectin mg/kg 0.01 Max

Meloxicam mg/kg 0.01 Max

Febantel mg/kg 0.1 Max

Fenbendazole mg/kg 0.1 Max

Oxyfendazole mg/kg 0.1 Max

Oxyclozanide mg/kg 0.01 Max

Sulphachloropyrazine mg/kg 0.01 Max

Parbendazole mg/kg 0.01 Max

Praziquantel mg/kg 0.01 Max

Thiabendazole mg/kg 0.1 Max

Diminazene mg/kg 0.15 Max

Cefphactril mg/kg 0.01 Max

BANNED ANTIBIOTICS (As per FSSA, 2006 and Rules & Regulations 2011)

Carbadox mg/kg ND

Chloramphenicol mg/kg ND

Chlorpromazine mg/kg ND

Clenbuterol mg/kg ND

Colistin mg/kg ND

Crystal Violet (Sum of Crystal Violet and Leucocrystal Violet) mg/kg ND

Glycopeptides mg/kg ND

Malachite Green (Sum of Malachite green and Leucomalachite green) mg/kg ND

Nitrofurans and its metabolites furazolidone (AOZ), nitrofurazone (SEM), furaltadone (AMOZ) and nitrofurantoin (AHD) mg/kg ND

Streptomycin and its metabolite dihydrostreptomycin mg/kg ND

Nitroimidazoles including- mg/kg ND

Dimetridazole (DMZ) mg/kg ND

Ronidazole (RNZ) and its metabolite 2-hydroxymethyl-1-methyl-3 nitroimidazole(HMMNI) mg/kg ND

Ipronidazole (IPZ) and its metabolite Hydroxyipronidazole mg/kg ND

Metronidazole (MNZ) and its metabolite 3 hydroxymetronidazole mg/kg ND

Steroids mg/kg ND

Stilbenes mg/kg ND

Sulphamethoxazole mg/kg ND

5 Frozen Yoghurt (Probiotic) Fat% Mini 8% DGHS and FSSAI: Pearson’s Composition and analysis of foods 9th edn,1991 page 604

Total Solid% Mini 32% DGHS and FSSAI: I.S 2802–1964 –Specification for Ice cream / Pearson’s Composition and analysis of foods, 9thedn, 1991 page 604

Acidity 0.45-0.55 %LA FSSAI: IS 1166 – 1973 Specification for condensed milk. Bureau of Indian Standards, New Delhi

Sucrose/Sugar 11.30-12.70 FSSAI: Lane-Eynon (Volumetric ) Method: IS 4079 – 1967(Reaffirmed 1995)Specification for canned rasogolla. Bureau of Indian Standards, New Delhi

Protein, min. 3.7 % min DGHS: Pearson’s Composition and Analysis of Foods, 9th edn, 1991 page 17.

Ash Contents AOAC 945.46 19th edition: 2012 AOAC 930.30 19 thedition: 2012

Total Colour Contents in Ice Cream, ppm Max 100 As per FSSAI

Microorganism (As per FSSA, 2006 and Rules & Regulations 2011)

Probiotic count per serving mini 10^8 cfu

TPC in 1 gm NMT 1,00,000

Coliform count in 1 gm NMT 10

E. coli in 1 gm Absent

Shigella in 25 gm Absent

Salmonella in 25gm Absent

S. aureus in 1 gm NMT 10

Listeria monocytogens in 1 gm Absent

Total Aflatoxin µg/kg 15

Melamine mg/kg 2.5 Max

Lead as Pb mg/kg Max 0.02

Copper as Cu mg/kg Max 30

Arsenic as As mg/kg Max 0.1

Tin mg/kg Max 250

Cadmium as Cd mg/kg Max 0.02

Mercury mg/kg Max 1

Methyl Mercury mg/kg Max 0.25

Nickel (Ni) mg/kg Max 0.2

Chromium (Cr) mg/kg Max 1.0

Nutritional Value per 100mL (approx value) As per Declaration

Energy, kcl As per Variety

Saturated Fat, g

Total carbohydrate, g

Insecticides & Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

2,4-Dichlorophenoxy Acetic Acid mg/kg 0.05 Max

Acephate (expressed as mixture of Methamidophos and acephate) mg/kg 0.02 Max

Acetamiprid mg/kg 0.02 Max

Azoxystrobin mg/kg 0.01 Max

Sum of benomyl and carbendazim expressed as carbendazim mg/kg 0.1 Max

Bifenthrin mg/kg 0.2 Max

Bitertanol mg/kg 0.05 Max

Buprofezin mg/kg 0.01 Max

Carbaryl mg/kg 0.05 Max

Carbendazim mg/kg 0.1 Max

Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran) mg/kg 0.05 Max

Chlorantraniliprole mg/kg 0.05 Max

Chlorothalonil mg/kg 0.07 Max

Chlorpyriphos mg/kg 0.02 Max

Chlothianidin (Chlothianidin and its metabolites Thiazolymethylguanidine (TMG), Thiazolymethylurea (TZMU), Methylnitroguanidine (MNG) TMG) mg/kg 0.02 Max

Cypermethrin (sum of isomers) (Fat soluble residue) mg/kg 0.05 Max

Deltamethrin (Decamethrin) mg/kg 0.05 Max

Dichlorvos (DDVP) (content ofdichloroacetaldehyde (D.C.A.) be reported where possible) mg/kg 0.01 Max

Difenoconazole mg/kg 0.02 Max

Dimethoate mg/kg 0.05 Max

Dinotefuran mg/kg 0.1 Max

Mancozeb mg/kg 0.05 Max

Metiram as CS2 mg/kg 0.05 Max

Edifenphos mg/kg 0.01 Max

Emamectin Benzoate mg/kg 0.01 Max

Ethion(Residues to be determined as ethion and its oxygen analogue and expressed as ethion) mg/kg 0.5 Max

Ethofenprox (Etofenprox) mg/kg 0.02 Max

Fenpropathrin mg/kg 0.1 Max

Fenvalerate (Fat soluble residue) mg/kg 0.01 Max

Fipronil mg/kg 0.02 Max

Flubendiamide mg/kg 0.1 Max

Flusilazole mg/kg 0.05 Max

Glufosinate Ammonium mg/kg 0.02 Max

Imidacloprid mg/kg 0.1 Max

Indoxacarb mg/kg 0.1 Max

Kresoxim Methyl mg/kg 0.01 Max

Methomyl mg/kg 0.02 Max

Methyl Chlorophenoxy Acetic Acid (MCPA) mg/kg 0.04 Max

Metolachlor mg/kg 0.01 Max

Monocrotophos mg/kg 0.02 Max

Oxydemeton-Methyl mg/kg 0.01 Max

Paraquat dichloride (Determined as Paraquatcations) mg/kg 0.01 Max

Penconazole mg/kg 0.01 Max

Phenthoate mg/kg 0.01 Max

Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate) mg/kg 0.05 Max

Pirimiphos-methyl mg/kg 0.05 Max

Propiconazole mg/kg 0.01 Max

Pyraclostrobin mg/kg 0.03 Max

Tebuconazole mg/kg 0.01 Max

Thiacloprid mg/kg 0.05 Max

Thiamethoxam mg/kg 0.05 Max

Thiophanate-Methyl mg/kg 0.05 Max

Trichlorfon mg/kg 0.05 Max

Triacontanol mg/kg 0.01 Max

Triadimefon mg/kg 0.01 Max

Banned Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

Aldicarb mg/kg ND

Aldrin mg/kg ND

Dieldrin mg/kg ND

Chlordane mg/kg ND

Heptachlor mg/kg ND

Lindane (Gamma-HCH) mg/kg ND

Endosulfan mg/kg ND

Phosphamidon mg/kg ND

Captafol mg/kg ND

Formothion mg/kg ND

Simazine mg/kg ND

Diazinon mg/kg ND

2,4 DDT mg/kg ND

4,4 DDT mg/kg ND

2,4 DDD mg/kg ND

4,4 DDD mg/kg ND

2,4 DDE mg/kg ND

4,4 DDE mg/kg ND

Fenitrothion mg/kg ND

Fenthion mg/kg ND

Methyl Parathion mg/kg ND

Ethyl Parathion mg/kg ND

Ferbam as CS2 mg/kg ND

Antibiotics (As per FSSA, 2006 and Rules & Regulations 2011)

Ampicillin mg/kg 0.01 Max

Chlortetracycline mg/kg 0.1 Max

Oxytetracycline mg/kg 0.1 Max

Tetracycline mg/kg 0.1 Max

Lincomycin mg/kg 0.15 Max

Neomycin mg/kg 1.5 Max

Spectinomycin mg/l 0.2 Max

Trimethoprim mg/kg 0.01 Max

Sulfadiazine mg/kg 0.01 Max

Sulfanilamide mg/kg 0.01 Max

Apramycin mg/kg 0.01 Max

Ceftiofur, mg/l mg/l 0.1 Max

Monensi mg/kg 0.002 Max

Sulphaquinoxaline mg/kg 0.01 Max

Sulfadimidine mg/kg 0.025 Max

Tylosin mg/kg 0.1 Max

Virginiamycin mg/kg 0.01 Max

Albendazole mg/kg 0.1 Max

Doramectin mg/kg 0.015 Max

Flunixin mg/kg 0.01 Max

Ivermectin mg/kg 0.01 Max

Meloxicam mg/kg 0.01 Max

Febantel mg/kg 0.1 Max

Fenbendazole mg/kg 0.1 Max

Oxyfendazole mg/kg 0.1 Max

Oxyclozanide mg/kg 0.01 Max

Sulphachloropyrazine mg/kg 0.01 Max

Parbendazole mg/kg 0.01 Max

Praziquantel mg/kg 0.01 Max

Thiabendazole mg/kg 0.1 Max

Diminazene mg/kg 0.15 Max

Cefphactril mg/kg 0.01 Max

BANNED ANTIBIOTICS (As per FSSA, 2006 and Rules & Regulations 2011)

Carbadox mg/kg ND

Chloramphenicol mg/kg ND

Chlorpromazine mg/kg ND

Clenbuterol mg/kg ND

Colistin mg/kg ND

Crystal Violet (Sum of Crystal Violet and Leucocrystal Violet) mg/kg ND

Glycopeptides mg/kg ND

Malachite Green (Sum of Malachite green and Leucomalachite green) mg/kg ND

Nitrofurans and its metabolites furazolidone (AOZ), nitrofurazone (SEM), furaltadone (AMOZ) and nitrofurantoin (AHD) mg/kg ND

Streptomycin and its metabolite dihydrostreptomycin mg/kg ND

Nitroimidazoles including- mg/kg ND

Dimetridazole (DMZ) mg/kg ND

Ronidazole (RNZ) and its metabolite 2-hydroxymethyl-1-methyl-3 nitroimidazole(HMMNI) mg/kg ND

Ipronidazole (IPZ) and its metabolite Hydroxyipronidazole mg/kg ND

Metronidazole (MNZ) and its metabolite 3 hydroxymetronidazole mg/kg ND

Steroids mg/kg ND

Stilbenes mg/kg ND

Sulphamethoxazole mg/kg ND

6 Ice Candy ( Ice Lickz -different flavour) Brix(Degree) 24-25

Total Solids %, Min 25% DGHS and FSSAI: I.S 2802–1964 –Specification for Ice cream / Pearson’s Composition and analysis of foods, 9thedn, 1991 page 604

Acidity % CA 0.32 - 0.40 % FSSAI: IS 1166 – 1973 Specification for condensed milk. Bureau of Indian Standards, New Delhi

Ash Contents Not specified AOAC 945.46 19th edition: 2012 AOAC 930.30 19 thedition: 2012

Total Colour Contents in Ice Cream, ppm Max 100 ppm As per FSSAI

Microorganism (As per FSSA, 2006 and Rules & Regulations 2011)

TPC in 1 gm NMT 1,00,000

Coliform count in 1 gm NMT 10

E. coli in 1 gm Absent

Shigella in 25 gm Absent

Salmonella in 25gm Absent

S. aureus in 1 gm NMT 10

Yeast and Mould in 1 gm NA

Listeria monocytogens in 1 gm Absent

Total Aflatoxin µg/kg 15

Melamine mg/kg 2.5 Max

Lead as Pb mg/kg Max 0.02

Copper as Cu mg/kg Max 30

Arsenic as As mg/kg Max 0.1

Tin mg/kg Max 250

Cadmium as Cd mg/kg Max 0.02

Mercury mg/kg Max 1

Methyl Mercury mg/kg Max 0.25

Nickel (Ni) mg/kg Max 0.2

Chromium (Cr) mg/kg Max 1.0

Nutritional Value per 100mL (approx value) As per Declaration

Energy, kcl As per Variety

Saturated Fat, g

Total carbohydrate, g

Insecticides & Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

2,4-Dichlorophenoxy Acetic Acid mg/kg 0.05 Max

Acephate (expressed as mixture of Methamidophos and acephate) mg/kg 0.02 Max

Acetamiprid mg/kg 0.02 Max

Azoxystrobin mg/kg 0.01 Max

Sum of benomyl and carbendazim expressed as carbendazim mg/kg 0.1 Max

Bifenthrin mg/kg 0.2 Max

Bitertanol mg/kg 0.05 Max

Buprofezin mg/kg 0.01 Max

Carbaryl mg/kg 0.05 Max

Carbendazim mg/kg 0.1 Max

Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran) mg/kg 0.05 Max

Chlorantraniliprole mg/kg 0.05 Max

Chlorothalonil mg/kg 0.07 Max

Chlorpyriphos mg/kg 0.02 Max

Chlothianidin (Chlothianidin and its metabolites Thiazolymethylguanidine (TMG), Thiazolymethylurea (TZMU), Methylnitroguanidine (MNG) TMG) mg/kg 0.02 Max

Cypermethrin (sum of isomers) (Fat soluble residue) mg/kg 0.05 Max

Deltamethrin (Decamethrin) mg/kg 0.05 Max

Dichlorvos (DDVP) (content ofdichloroacetaldehyde (D.C.A.) be reported where possible) mg/kg 0.01 Max

Difenoconazole mg/kg 0.02 Max

Dimethoate mg/kg 0.05 Max

Dinotefuran mg/kg 0.1 Max

Mancozeb mg/kg 0.05 Max

Metiram as CS2 mg/kg 0.05 Max

Edifenphos mg/kg 0.01 Max

Emamectin Benzoate mg/kg 0.01 Max

Ethion(Residues to be determined as ethion and its oxygen analogue and expressed as ethion) mg/kg 0.5 Max

Ethofenprox (Etofenprox) mg/kg 0.02 Max

Fenpropathrin mg/kg 0.1 Max

Fenvalerate (Fat soluble residue) mg/kg 0.01 Max

Fipronil mg/kg 0.02 Max

Flubendiamide mg/kg 0.1 Max

Flusilazole mg/kg 0.05 Max

Glufosinate Ammonium mg/kg 0.02 Max

Imidacloprid mg/kg 0.1 Max

Indoxacarb mg/kg 0.1 Max

Kresoxim Methyl mg/kg 0.01 Max

Methomyl mg/kg 0.02 Max

Methyl Chlorophenoxy Acetic Acid (MCPA) mg/kg 0.04 Max

Metolachlor mg/kg 0.01 Max

Monocrotophos mg/kg 0.02 Max

Oxydemeton-Methyl mg/kg 0.01 Max

Paraquat dichloride (Determined as Paraquatcations) mg/kg 0.01 Max

Penconazole mg/kg 0.01 Max

Phenthoate mg/kg 0.01 Max

Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate) mg/kg 0.05 Max

Pirimiphos-methyl mg/kg 0.05 Max

Propiconazole mg/kg 0.01 Max

Pyraclostrobin mg/kg 0.03 Max

Tebuconazole mg/kg 0.01 Max

Thiacloprid mg/kg 0.05 Max

Thiamethoxam mg/kg 0.05 Max

Thiophanate-Methyl mg/kg 0.05 Max

Trichlorfon mg/kg 0.05 Max

Triacontanol mg/kg 0.01 Max

Triadimefon mg/kg 0.01 Max

Banned Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

Aldicarb mg/kg ND

Aldrin mg/kg ND

Dieldrin mg/kg ND

Chlordane mg/kg ND

Heptachlor mg/kg ND

Lindane (Gamma-HCH) mg/kg ND

Endosulfan mg/kg ND

Phosphamidon mg/kg ND

Captafol mg/kg ND

Formothion mg/kg ND

Simazine mg/kg ND

Diazinon mg/kg ND

2,4 DDT mg/kg ND

4,4 DDT mg/kg ND

2,4 DDD mg/kg ND

4,4 DDD mg/kg ND

2,4 DDE mg/kg ND

4,4 DDE mg/kg ND

Fenitrothion mg/kg ND

Fenthion mg/kg ND

Methyl Parathion mg/kg ND

Ethyl Parathion mg/kg ND

Ferbam as CS2 mg/kg ND

Antibiotics (As per FSSA, 2006 and Rules & Regulations 2011)

Ampicillin mg/kg 0.01 Max

Chlortetracycline mg/kg 0.1 Max

Oxytetracycline mg/kg 0.1 Max

Tetracycline mg/kg 0.1 Max

Lincomycin mg/kg 0.15 Max

Neomycin mg/kg 1.5 Max

Spectinomycin mg/l 0.2 Max

Trimethoprim mg/kg 0.01 Max

Sulfadiazine mg/kg 0.01 Max

Sulfanilamide mg/kg 0.01 Max

Apramycin mg/kg 0.01 Max

Ceftiofur, mg/l mg/l 0.1 Max

Monensi mg/kg 0.002 Max

Sulphaquinoxaline mg/kg 0.01 Max

Sulfadimidine mg/kg 0.025 Max

Tylosin mg/kg 0.1 Max

Virginiamycin mg/kg 0.01 Max

Albendazole mg/kg 0.1 Max

Doramectin mg/kg 0.015 Max

Flunixin mg/kg 0.01 Max

Ivermectin mg/kg 0.01 Max

Meloxicam mg/kg 0.01 Max

Febantel mg/kg 0.1 Max

Fenbendazole mg/kg 0.1 Max

Oxyfendazole mg/kg 0.1 Max

Oxyclozanide mg/kg 0.01 Max

Sulphachloropyrazine mg/kg 0.01 Max

Parbendazole mg/kg 0.01 Max

Praziquantel mg/kg 0.01 Max

Thiabendazole mg/kg 0.1 Max

Diminazene mg/kg 0.15 Max

Cefphactril mg/kg 0.01 Max

BANNED ANTIBIOTICS (As per FSSA, 2006 and Rules & Regulations 2011)

Carbadox mg/kg ND

Chloramphenicol mg/kg ND

Chlorpromazine mg/kg ND

Clenbuterol mg/kg ND

Colistin mg/kg ND

Crystal Violet (Sum of Crystal Violet and Leucocrystal Violet) mg/kg ND

Glycopeptides mg/kg ND

Malachite Green (Sum of Malachite green and Leucomalachite green) mg/kg ND

Nitrofurans and its metabolites furazolidone (AOZ), nitrofurazone (SEM), furaltadone (AMOZ) and nitrofurantoin (AHD) mg/kg ND

Streptomycin and its metabolite dihydrostreptomycin mg/kg ND

Nitroimidazoles including- mg/kg ND

Dimetridazole (DMZ) mg/kg ND

Ronidazole (RNZ) and its metabolite 2-hydroxymethyl-1-methyl-3 nitroimidazole(HMMNI) mg/kg ND

Ipronidazole (IPZ) and its metabolite Hydroxyipronidazole mg/kg ND

Metronidazole (MNZ) and its metabolite 3 hydroxymetronidazole mg/kg ND

Steroids mg/kg ND

Stilbenes mg/kg ND

Sulphamethoxazole mg/kg ND

7 Ice Cream (Plain/Nut variety) Fat As per variety DGHS and FSSAI: Pearson’s Composition and analysis of foods 9th edn,1991 page 604

Total Solids %, Min As per variety DGHS and FSSAI: I.S 2802–1964 –Specification for Ice cream / Pearson’s Composition and analysis of foods, 9thedn, 1991 page 604

Acidity 0.180 max FSSAI: IS 1166 – 1973 Specification for condensed milk. Bureau of Indian Standards, New Delhi

Protein 3.75-3.95 DGHS: Pearson’s Composition and Analysis of Foods, 9th edn, 1991 page 17.

Sucrose 15-16% FSSAI: Lane-Eynon (Volumetric ) Method: IS 4079 – 1967(Reaffirmed 1995)Specification for canned rasogolla. Bureau of Indian Standards, New Delhi

Over Run In Ice Cream 90% min FSSAI: IS:2802: 1964 (Reaffirmed 1995) Specification for ice-cream. Bureau of Indian Standards, New Delhi

Ash Contents Not specified AOAC 945.46 19th edition: 2012 AOAC 930.30 19 thedition: 2012

Nut Content As per variety As per GCMMF

Total Colour Contents in Ice Cream, ppm 100ppm As per FSSAI

Microorganism (As per FSSA, 2006 and Rules & Regulations 2011)

TPC in 1 gm NMT 1,00,000

Coliform count in 1 gm NMT 10

E. coli in 1 gm Absent

Shigella in 25 gm -

Salmonella in 25gm Absent

S. aureus in 1 gm NMT 10

Yeast and Mould in 1 gm NA

Listeria monocytogens in 1 gm Absent

Total Aflatoxin µg/kg 15 (Plain) & 20 (Nut)

Melamine mg/kg 2.5 Max

Lead as Pb mg/kg Max 0.02

Copper as Cu mg/kg Max 30

Arsenic as As mg/kg Max 0.1

Tin mg/kg Max 250

Cadmium as Cd mg/kg Max 0.02

Mercury mg/kg Max 1

Methyl Mercury mg/kg Max 0.25

Nickel (Ni) mg/kg Max 0.2

Chromium (Cr) mg/kg Max 1.0

Nutritional Value per 100mL (approx value) As per Declaration

Energy, kcl As per Variety

Saturated Fat, g

Total carbohydrate, g

Insecticides & Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

2,4-Dichlorophenoxy Acetic Acid mg/kg 0.05 Max

Acephate (expressed as mixture of Methamidophos and acephate) mg/kg 0.02 Max

Acetamiprid mg/kg 0.02 Max

Azoxystrobin mg/kg 0.01 Max

Sum of benomyl and carbendazim expressed as carbendazim mg/kg 0.1 Max

Bifenthrin mg/kg 0.2 Max

Bitertanol mg/kg 0.05 Max

Buprofezin mg/kg 0.01 Max

Carbaryl mg/kg 0.05 Max

Carbendazim mg/kg 0.1 Max

Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran) mg/kg 0.05 Max

Chlorantraniliprole mg/kg 0.05 Max

Chlorothalonil mg/kg 0.07 Max

Chlorpyriphos mg/kg 0.02 Max

Chlothianidin (Chlothianidin and its metabolites Thiazolymethylguanidine (TMG), Thiazolymethylurea (TZMU), Methylnitroguanidine (MNG) TMG) mg/kg 0.02 Max

Cypermethrin (sum of isomers) (Fat soluble residue) mg/kg 0.05 Max

Deltamethrin (Decamethrin) mg/kg 0.05 Max

Dichlorvos (DDVP) (content ofdichloroacetaldehyde (D.C.A.) be reported where possible) mg/kg 0.01 Max

Difenoconazole mg/kg 0.02 Max

Dimethoate mg/kg 0.05 Max

Dinotefuran mg/kg 0.1 Max

Mancozeb mg/kg 0.05 Max

Metiram as CS2 mg/kg 0.05 Max

Edifenphos mg/kg 0.01 Max

Emamectin Benzoate mg/kg 0.01 Max

Ethion(Residues to be determined as ethion and its oxygen analogue and expressed as ethion) mg/kg 0.5 Max

Ethofenprox (Etofenprox) mg/kg 0.02 Max

Fenpropathrin mg/kg 0.1 Max

Fenvalerate (Fat soluble residue) mg/kg 0.01 Max

Fipronil mg/kg 0.02 Max

Flubendiamide mg/kg 0.1 Max

Flusilazole mg/kg 0.05 Max

Glufosinate Ammonium mg/kg 0.02 Max

Imidacloprid mg/kg 0.1 Max

Indoxacarb mg/kg 0.1 Max

Kresoxim Methyl mg/kg 0.01 Max

Methomyl mg/kg 0.02 Max

Methyl Chlorophenoxy Acetic Acid (MCPA) mg/kg 0.04 Max

Metolachlor mg/kg 0.01 Max

Monocrotophos mg/kg 0.02 Max

Oxydemeton-Methyl mg/kg 0.01 Max

Paraquat dichloride (Determined as Paraquatcations) mg/kg 0.01 Max

Penconazole mg/kg 0.01 Max

Phenthoate mg/kg 0.01 Max

Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate) mg/kg 0.05 Max

Pirimiphos-methyl mg/kg 0.05 Max

Propiconazole mg/kg 0.01 Max

Pyraclostrobin mg/kg 0.03 Max

Tebuconazole mg/kg 0.01 Max

Thiacloprid mg/kg 0.05 Max

Thiamethoxam mg/kg 0.05 Max

Thiophanate-Methyl mg/kg 0.05 Max

Trichlorfon mg/kg 0.05 Max

Triacontanol mg/kg 0.01 Max

Triadimefon mg/kg 0.01 Max

Banned Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

Aldicarb mg/kg ND

Aldrin mg/kg ND

Dieldrin mg/kg ND

Chlordane mg/kg ND

Heptachlor mg/kg ND

Lindane (Gamma-HCH) mg/kg ND

Endosulfan mg/kg ND

Phosphamidon mg/kg ND

Captafol mg/kg ND

Formothion mg/kg ND

Simazine mg/kg ND

Diazinon mg/kg ND

2,4 DDT mg/kg ND

4,4 DDT mg/kg ND

2,4 DDD mg/kg ND

4,4 DDD mg/kg ND

2,4 DDE mg/kg ND

4,4 DDE mg/kg ND

Fenitrothion mg/kg ND

Fenthion mg/kg ND

Methyl Parathion mg/kg ND

Ethyl Parathion mg/kg ND

Ferbam as CS2 mg/kg ND

Antibiotics (As per FSSA, 2006 and Rules & Regulations 2011)

Ampicillin mg/kg 0.01 Max

Chlortetracycline mg/kg 0.1 Max

Oxytetracycline mg/kg 0.1 Max

Tetracycline mg/kg 0.1 Max

Lincomycin mg/kg 0.15 Max

Neomycin mg/kg 1.5 Max

Spectinomycin mg/l 0.2 Max

Trimethoprim mg/kg 0.01 Max

Sulfadiazine mg/kg 0.01 Max

Sulfanilamide mg/kg 0.01 Max

Apramycin mg/kg 0.01 Max

Ceftiofur, mg/l mg/l 0.1 Max

Monensi mg/kg 0.002 Max

Sulphaquinoxaline mg/kg 0.01 Max

Sulfadimidine mg/kg 0.025 Max

Tylosin mg/kg 0.1 Max

Virginiamycin mg/kg 0.01 Max

Albendazole mg/kg 0.1 Max

Doramectin mg/kg 0.015 Max

Flunixin mg/kg 0.01 Max

Ivermectin mg/kg 0.01 Max

Meloxicam mg/kg 0.01 Max

Febantel mg/kg 0.1 Max

Fenbendazole mg/kg 0.1 Max

Oxyfendazole mg/kg 0.1 Max

Oxyclozanide mg/kg 0.01 Max

Sulphachloropyrazine mg/kg 0.01 Max

Parbendazole mg/kg 0.01 Max

Praziquantel mg/kg 0.01 Max

Thiabendazole mg/kg 0.1 Max

Diminazene mg/kg 0.15 Max

Cefphactril mg/kg 0.01 Max

BANNED ANTIBIOTICS (As per FSSA, 2006 and Rules & Regulations 2011)

Carbadox mg/kg ND

Chloramphenicol mg/kg ND

Chlorpromazine mg/kg ND

Clenbuterol mg/kg ND

Colistin mg/kg ND

Crystal Violet (Sum of Crystal Violet and Leucocrystal Violet) mg/kg ND

Glycopeptides mg/kg ND

Malachite Green (Sum of Malachite green and Leucomalachite green) mg/kg ND

Nitrofurans and its metabolites furazolidone (AOZ), nitrofurazone (SEM), furaltadone (AMOZ) and nitrofurantoin (AHD) mg/kg ND

Streptomycin and its metabolite dihydrostreptomycin mg/kg ND

Nitroimidazoles including- mg/kg ND

Dimetridazole (DMZ) mg/kg ND

Ronidazole (RNZ) and its metabolite 2-hydroxymethyl-1-methyl-3 nitroimidazole(HMMNI) mg/kg ND

Ipronidazole (IPZ) and its metabolite Hydroxyipronidazole mg/kg ND

Metronidazole (MNZ) and its metabolite 3 hydroxymetronidazole mg/kg ND

Steroids mg/kg ND

Stilbenes mg/kg ND

Sulphamethoxazole mg/kg ND

8 Raw Milk Reichert-Meissl Value (extracted fat) min 28 FSSAI : IS 3508 – 1966 (Reaffirmed 1997) Methods of sampling and test for Ghee (Butterfat). Bureau of Indian Standards, New Delhi

BR Test 40 -43 FSSAI: IS 3508 – 1966 (Reaffirmed 1997) Methods of sampling and test for Ghee (Butterfat). Bureau of Indian Standards, New Delhi; Kumar, A.; Lal, D.; Seth, R. and Sharma, R.(2002) Recent trends in detection of adulteration in milk fat: a review: Indian J. Dairy Sci., 55 (6): 319-330. Rangappa, K.S. and Achaya, K.T. 1974. In: Indian Dairy Products. Asia Pub. House, Bombay

Mineral Oil Test Negative DGHS and FSSAI: I.S.I. Handbook of Food Analysis (Part XIII)-1984 Page 89/ A.O.A.C 17th edn, 2000, Official Method 945.102 – Oil (mineral) in fats –Qualitative Test

Animal fats & Vegetable oils/fats (By Valenta and Hager Test) Negative Handbook on Analysis of Milk, Page No. 154

Sugar Test Negative FSSAI: IS 1479 ( Part I) 1961 (Reaffirmed 2003) Methods of test for Dairy Industry – Rapid Examination of Milk. Bureau of Indian Standards, New Delhi

Rosalic Acid Test/ Detection of Neutralizers Negative DGHS & FSSAI: IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi

Starch Test Negative DGHS & FSSAI: I.S.1479 (Part I) – 1960 Methods of test for Dairy Industry, Rapid examination of Milk

Salt Test Negative DGHS & FSSAI: Pearson’s Composition and Analysis of Foods, 9thedn,1991 – Modified Mohr method, page 14

Urea Test (Qualitative ) Negative NDDB, Technews, Nov-Dec 2009,No. 83

Urea Test (Quantitative ) 700 ppm max DGHS : A.O.A.C 17th edn, 2000 Modified Official method 967.07, Urea in animal feed

Nitrates (Pond Water) Test Negative FSSAI: Sharma, R.; Rajput, Y.S. and Naik, N.L. (2012). Detection of adulterants in milk – a laboratory manual. NDRI Publication No. 88/2012, NDRI, Karnal, page 47-48

Sodium Thiosulphate Negative Handbook on Analysis of Milk, Page No. 122

Ammonium Compounds Negative Handbook on Analysis of Milk,Page No. 133

Ammonium Sulphate Negative DGHS & FSSAI: Milk and Milk products Vol. 5 Published by N.C.E.R.T

Cellulose Negative FSSAI: Manual Methods of Analysis for Adulterants & Contaminants in Foods. I.C.M.R 1990

Formalin in Milk Negative DGHS & FSSAI: Method 1:Hehner’s Test: Pearson’s Composition and Analysis of foods, 9th edition, 1991 page 90; IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi

Boric acid and Borates Negative FSSAI: Method 1 & 2: IS 1479 ( Part I) 1961 (Reaffirmed 2003) Methods of test for Dairy Industry – Rapid Examination of Milk. Bureau of Indian Standards, New Delhi

Detection of Hypochlorites Negative DGHS & FSSAI : IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi; A.O.A.C 17th edn, 2000 Official Method 922.08 Hypochlorites and Chloramines in milk

Detection of Maltodextrin Negative FSSAI: IS 1479 (Part II) 1961 (Reaffirmed 1997, being revised) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi.

Detection and Estimation of Added Glucose in Milk Negative DGHS & FSSAI: Manual Methods of Analysis for Adulterants and Contaminants in Foods, I.C.M.R 1990, page 28; Roy, N.K. and Sen, D.C. (1991) Rapid analysis of milk. In: Textbook of Practical Dairy Chemistry. Vol. I. Chemical analysis of fluid milk. Kalyani Publishers, New Delhi, India

Anionic Detergent in Milk Negative FSSAI: Rajput, Y.S.; Sharma, R. and Kaur, S. (2006) A kit for detection of detergent in milk. Indian Patent Office file no. 1970/Del/2006.

Presence of Skimmed milk Powder in Natural milk Absent FSSAI: Journal of Food Science and Technology, Vol 22 (1985) page 207-208

Detection of Gelatine in Milk Absent FSSAI: A.O.A.C 17thedn ,2000 Official Method - 920.106. Gelatine in Milk and Milk products

Presence of Hydrogen Peroxide in Milk Absent FSSAI: Method 1: Vanadium pentoxide Test: A.O.A.C 17thedn, 2000 Official Method 957.08 Hydrogen Peroxide in milk

Salicylic acid in Milk Absent FSSAI: A.O.A.C 17th, edn Official method 975. 30 Salicylic acid in Food and Beverages / IS 1479 ( Part II) 1961 (Reaffirmed 1997) Methods of test for Dairy Industry – Chemical Analysis of Milk. Bureau of Indian Standards, New Delhi).

Beta Sitosterol Absent As per FSSAI

Microorganism (As per FSSA, 2006 and Rules & Regulations 2011)

Somatic Cell Count in 1 ml ≤ 400000

Aflatoxin M1 , MAX µg/kg 0.5

Melamine mg/kg 2.5 Max

Lead as Pb mg/kg Max 0.02

Copper as Cu mg/kg Max 30

Arsenic as As mg/kg Max 0.1

Tin mg/kg Max 250

Cadmium as Cd mg/kg Max 0.02

Mercury mg/kg Max 1

Methyl Mercury mg/kg Max 0.25

Nickel (Ni) mg/kg Max 0.2

Chromium (Cr) mg/kg Max 1.0

Insecticides & Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

2,4-Dichlorophenoxy Acetic Acid mg/kg 0.05 Max

Acephate (expressed as mixture of Methamidophos and acephate) mg/kg 0.02 Max

Acetamiprid mg/kg 0.02 Max

Azoxystrobin mg/kg 0.01 Max

Sum of benomyl and carbendazim expressed as carbendazim mg/kg 0.1 Max

Bifenthrin mg/kg 0.2 Max

Bitertanol mg/kg 0.05 Max

Buprofezin mg/kg 0.01 Max

Carbaryl mg/kg 0.05 Max

Carbendazim mg/kg 0.1 Max

Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran) mg/kg 0.05 Max

Chlorantraniliprole mg/kg 0.05 Max

Chlorothalonil mg/kg 0.07 Max

Chlorpyriphos mg/kg 0.02 Max

Chlothianidin (Chlothianidin and its metabolites Thiazolymethylguanidine (TMG), Thiazolymethylurea (TZMU), Methylnitroguanidine (MNG) TMG) mg/kg 0.02 Max

Cypermethrin (sum of isomers) (Fat soluble residue) mg/kg 0.05 Max

Deltamethrin (Decamethrin) mg/kg 0.05 Max

Dichlorvos (DDVP) (content ofdichloroacetaldehyde (D.C.A.) be reported where possible) mg/kg 0.01 Max

Difenoconazole mg/kg 0.02 Max

Dimethoate mg/kg 0.05 Max

Dinotefuran mg/kg 0.1 Max

Mancozeb mg/kg 0.05 Max

Metiram as CS2 mg/kg 0.05 Max

Edifenphos mg/kg 0.01 Max

Emamectin Benzoate mg/kg 0.01 Max

Ethion(Residues to be determined as ethion and its oxygen analogue and expressed as ethion) mg/kg 0.5 Max

Ethofenprox (Etofenprox) mg/kg 0.02 Max

Fenpropathrin mg/kg 0.1 Max

Fenvalerate (Fat soluble residue) mg/kg 0.01 Max

Fipronil mg/kg 0.02 Max

Flubendiamide mg/kg 0.1 Max

Flusilazole mg/kg 0.05 Max

Glufosinate Ammonium mg/kg 0.02 Max

Imidacloprid mg/kg 0.1 Max

Indoxacarb mg/kg 0.1 Max

Kresoxim Methyl mg/kg 0.01 Max

Methomyl mg/kg 0.02 Max

Methyl Chlorophenoxy Acetic Acid (MCPA) mg/kg 0.04 Max

Metolachlor mg/kg 0.01 Max

Monocrotophos mg/kg 0.02 Max

Oxydemeton-Methyl mg/kg 0.01 Max

Paraquat dichloride (Determined as Paraquatcations) mg/kg 0.01 Max

Penconazole mg/kg 0.01 Max

Phenthoate mg/kg 0.01 Max

Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate) mg/kg 0.05 Max

Pirimiphos-methyl mg/kg 0.05 Max

Propiconazole mg/kg 0.01 Max

Pyraclostrobin mg/kg 0.03 Max

Tebuconazole mg/kg 0.01 Max

Thiacloprid mg/kg 0.05 Max

Thiamethoxam mg/kg 0.05 Max

Thiophanate-Methyl mg/kg 0.05 Max

Trichlorfon mg/kg 0.05 Max

Triacontanol mg/kg 0.01 Max

Triadimefon mg/kg 0.01 Max

Banned Pesticides (As per FSSA, 2006 and Rules & Regulations 2011)

Aldicarb mg/kg ND

Aldrin mg/kg ND

Dieldrin mg/kg ND

Chlordane mg/kg ND

Heptachlor mg/kg ND

Lindane (Gamma-HCH) mg/kg ND

Endosulfan mg/kg ND

Phosphamidon mg/kg ND

Captafol mg/kg ND

Formothion mg/kg ND

Simazine mg/kg ND

Diazinon mg/kg ND

2,4 DDT mg/kg ND

4,4 DDT mg/kg ND

2,4 DDD mg/kg ND

4,4 DDD mg/kg ND

2,4 DDE mg/kg ND

4,4 DDE mg/kg ND

Fenitrothion mg/kg ND

Fenthion mg/kg ND

Methyl Parathion mg/kg ND

Ethyl Parathion mg/kg ND

Ferbam as CS2 mg/kg ND

Antibiotics (As per FSSA, 2006 and Rules & Regulations 2011)

Ampicillin mg/kg 0.01 Max

Chlortetracycline mg/kg 0.1 Max

Oxytetracycline mg/kg 0.1 Max

Tetracycline mg/kg 0.1 Max

Lincomycin mg/kg 0.15 Max

Neomycin mg/kg 1.5 Max

Spectinomycin mg/l 0.2 Max

Trimethoprim mg/kg 0.01 Max

Sulfadiazine mg/kg 0.01 Max

Sulfanilamide mg/kg 0.01 Max

Apramycin mg/kg 0.01 Max

Ceftiofur, mg/l mg/l 0.1 Max

Monensi mg/kg 0.002 Max

Sulphaquinoxaline mg/kg 0.01 Max

Sulfadimidine mg/kg 0.025 Max

Tylosin mg/kg 0.1 Max

Virginiamycin mg/kg 0.01 Max

Albendazole mg/kg 0.1 Max

Doramectin mg/kg 0.015 Max

Flunixin mg/kg 0.01 Max

Ivermectin mg/kg 0.01 Max

Meloxicam mg/kg 0.01 Max

Febantel mg/kg 0.1 Max

Fenbendazole mg/kg 0.1 Max

Oxyfendazole mg/kg 0.1 Max

Oxyclozanide mg/kg 0.01 Max

Sulphachloropyrazine mg/kg 0.01 Max

Parbendazole mg/kg 0.01 Max

Praziquantel mg/kg 0.01 Max

Thiabendazole mg/kg 0.1 Max

Diminazene mg/kg 0.15 Max

Cefphactril mg/kg 0.01 Max

BANNED ANTIBIOTICS (As per FSSA, 2006 and Rules & Regulations 2011)

Carbadox mg/kg ND

Chloramphenicol mg/kg ND

Chlorpromazine mg/kg ND

Clenbuterol mg/kg ND

Colistin mg/kg ND

Crystal Violet (Sum of Crystal Violet and Leucocrystal Violet) mg/kg ND

Glycopeptides mg/kg ND

Malachite Green (Sum of Malachite green and Leucomalachite green) mg/kg ND

Nitrofurans and its metabolites furazolidone (AOZ), nitrofurazone (SEM), furaltadone (AMOZ) and nitrofurantoin (AHD) mg/kg ND

Streptomycin and its metabolite dihydrostreptomycin mg/kg ND

Nitroimidazoles including- mg/kg ND

Dimetridazole (DMZ) mg/kg ND

Ronidazole (RNZ) and its metabolite 2-hydroxymethyl-1-methyl-3 nitroimidazole(HMMNI) mg/kg ND

Ipronidazole (IPZ) and its metabolite Hydroxyipronidazole mg/kg ND

Metronidazole (MNZ) and its metabolite 3 hydroxymetronidazole mg/kg ND

Steroids mg/kg ND

Stilbenes mg/kg ND

Sulphamethoxazole mg/kg ND

9 RT-PPCR Analysis of A1-A2 Milk

10 RT-PPCR Analysis of Cow-Buffalo Milk

S.N. Sample Description Test Parameters Unit Specified Norms Reference Rate (Basic)

1 Kaju Chikki Moisture Max.1.5% As per GCMMF

Coliform/g Max in 1 gm Absent As per GCMMF

Yeast & Mold Max in 1 gm Absent As per GCMMF

TPC in 1 gm Not more than 100000 As per FSSA, 2006 and Rules & Regulations 2011

S.aureus in 1 gm Not more than 100

Salmonella in 25 gm Absent

E.coli in 1 gm Absent

Lead (Pb) ppm Max 2.5

Arsenic as As ppm Max 1.1

Cadmium (Cd) ppm Max 1.0

Mercury (Hg) ppm Max 1.0

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Aflatoxin B1 ppb ≤ 5

Aflatoxin (Total) ppb ≤10

2 Kaju Moisture Max.5% As per GCMMF

Acidity of extracted fat as oleic acid Max.1.25%

TPC in 1 gm Not more than 40000 CFU

S.aureus in 25 gm Absent

Salmonella in 25 gm Absent

Shigella in 25 gm Absent

Clostridium Botulinm in 25 gm Absent

Vibrio Cholera in 25 gm Absent

E.coli in 1 gm Absent

Yeast & Mold Max in 1 gm NMT 1000 As per FSSA, 2006 and Rules & Regulations 2011

Lead (Pb) ppm Max 2.5

Arsenic as As ppm Max 1.1

Cadmium (Cd) ppm Max 1.0

Mercury (Hg) ppm Max 1.0

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Aflatoxin B1 ppb ≤ 5

Aflatoxin (Total) ppb ≤10

3 Kishmish (Raisins) Moisture Max.15% As per GCMMF

TPC in 1 gm Not more than 40000 CFU

S.aureus in 25 gm Absent

Salmonella in 25 gm Absent

Shigella in 25 gm Absent

Clostridium Botulinm in 25 gm Absent

Vibrio Cholera in 25 gm Absent

E.coli in 1 gm Absent

Yeast & Mold Max in 1 gm NMT 1000 As per FSSA, 2006 and Rules & Regulations 2011

Sulphur Dioxide ppm Max 2000

Lead (Pb) ppm Max 2.5

Arsenic as As ppm Max 1.1

Cadmium (Cd) ppm Max 1.0

Mercury (Hg) ppm Max 1.0

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Aflatoxin B1 ppb ≤ 5

Aflatoxin (Total) ppb ≤10

4 Anjir (Fig) Moisture Min 15% As per GCMMF

TPC in 1 gm Not more than 40000 CFU

S.aureus in 25 gm Absent

Salmonella in 25 gm Absent

Shigella in 25 gm Absent

Clostridium Botulinm in 25 gm Absent

Vibrio Cholera in 25 gm Absent

E.coli in 1 gm Absent

Yeast & Mold Max in 1 gm NMT 1000 As per FSSA, 2006 and Rules & Regulations 2011

Sulphur Dioxide ppm Max 2000

Lead (Pb) ppm Max 2.5

Arsenic as As ppm Max 1.1

Cadmium (Cd) ppm Max 1.0

Mercury (Hg) ppm Max 1.0

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Aflatoxin B1 ppb ≤ 5

Aflatoxin (Total) ppb ≤10

5 Pista Moisture Max 7% As per GCMMF

TPC in 1 gm Not more than 40000 CFU

S.aureus in 25 gm Absent

Salmonella in 25 gm Absent

Shigella in 25 gm Absent

Clostridium Botulinm in 25 gm Absent

Vibrio Cholera in 25 gm Absent

E.coli in 1 gm Absent

Yeast & Mold Max in 1 gm NMT 1000 As per FSSA, 2006 and Rules & Regulations 2011

Lead (Pb) ppm Max 2.5

Arsenic as As ppm Max 1.1

Cadmium (Cd) ppm Max 1.0

Mercury (Hg) ppm Max 1.0

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Aflatoxin B1 ppb ≤ 5

Aflatoxin (Total) ppb ≤10

6 Almond Moisture Max 5% As per GCMMF

Acidity of extracted fat as oleic acid Max.1.25%

TPC in 1 gm Not more than 40000 CFU

S.aureus in 25 gm Absent

Salmonella in 25 gm Absent

Shigella in 25 gm Absent

Clostridium Botulinm in 25 gm Absent

Vibrio Cholera in 25 gm Absent

E.coli in 1 gm Absent

Yeast & Mold Max in 1 gm NMT 1000 As per FSSA, 2006 and Rules & Regulations 2011

Lead (Pb) ppm Max 2.5

Arsenic as As ppm Max 1.1

Cadmium (Cd) ppm Max 1.0

Mercury (Hg) ppm Max 1.0

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Aflatoxin B1 ppb ≤ 5

Aflatoxin (Total) ppb ≤10

7 Dates (Khajur) Moisture Max 30% As per GCMMF

Ash insoluble in Dil. HCL NMT 0.1%

TPC in 1 gm Not more than 40000 CFU

S.aureus in 25 gm Absent

Salmonella in 25 gm Absent

Shigella in 25 gm Absent

Clostridium Botulinm in 25 gm Absent

Vibrio Cholera in 25 gm Absent

E.coli in 1 gm Absent

Yeast & Mold Max in 1 gm NMT 1000 As per FSSA, 2006 and Rules & Regulations 2011

Lead (Pb) ppm Max 2.5

Arsenic as As ppm Max 1.1

Cadmium (Cd) ppm Max 1.0

Mercury (Hg) ppm Max 1.0

Sulphur Dioxide ppm Max 2000

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Aflatoxin B1 ppb ≤ 5

Aflatoxin (Total) ppb ≤10

8 Tutti-Fruity Moisture Max 6% As per GCMMF

Total Sugar(w/w) NLT 70%

% Reducing sugar to total sugar NLT 25%

TPC in 1 gm Not more than 1000 CFU

S.aureus in 25 gm Absent

Salmonella in 25 gm Absent

Shigella in 25 gm Absent

Clostridium Botulinm in 25 gm Absent

Vibrio Cholera in 25 gm Absent

E.coli in 1 gm Absent

Yeast & Mold in 25 gm Absent As per FSSA, 2006 and Rules & Regulations 2011

Lead (Pb) ppm Max 2.5

Arsenic as As ppm Max 1.1

Cadmium (Cd) ppm Max 1.0

Mercury (Hg) ppm Max 1.0

Sulphur Dioxide ppm Max 2000

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Aflatoxin B1 ppb ≤ 5

Aflatoxin (Total) ppb ≤10

9 Pectin Degree of amidation,%by mass of total carboxyl group of pectin Max 25 As per FSSA, 2006 and Rules & Regulations 2011

Loss on Drying Max 12%

Methanol ,% by Mass Max 1

Ethanol ,% by Mass Max 1

2-Propanol ,% by Mass Max 1

Methanol , Ethanol & 2-Propanol ,% by Mass Max 1

Galacturonic Acid, % by mass on ash free and dried basis Min 65% (Dry basis)

Acid insoluble ash, % by mass Max 1

Total insolubles, % by mass Max 3

Nitrogen , % by mass Max 2.5

Lead As Pb ppm Max 2

Arsenic as As ppm Max 5

Copper as Cu ppm Max 300

Sulphur Dioxide ppm Max 50

Total Plate Count in 1 gm Max 1000

Yeast & mould in 1 gm Max 100

E.Coli in 1 gm Absent

Salmonella in 25 gm Absent

Staphylococcus aureus in 1 gm Absent

10 Kulfi Stabilizer Icoquell A/Stamulcol IC-GC112 /Stabilizer cum Emulsifier)/ Kreamaze 1400/Kreamaze 1000/Kreamaze Majik LF-2411/ Fruit O Freeze/Unicream 801 Loss on Drying Max 15% As per FSSA, 2006 and Rules & Regulations 2011

Methanol ,% by Mass Max 1

Ethanol ,% by Mass Max 1

2-Propanol ,% by Mass Max 1

Methanol , Ethanol & 2-Propanol ,% by Mass Max 1

Acid insoluble ash, % by mass Max 1

Total insolubles, % by mass Max 3

Lead As Pb ppm Max 2

Arsenic as As ppm Max 5

Copper as Cu ppm Max 300

Sulphur Dioxide ppm Max 50

Total Plate Count in 1 gm Max 1000

Yeast & mould in 1 gm Max 100

E.Coli in 1 gm Absent

Salmonella in 25 gm Absent

Staphylococcus aureus in 1 gm Absent

11 Saffron (Kesar) Added Colouring matter Absent As per FSSA, 2006 and Rules & Regulations 2011

Moisture & volatile matter at 103'C % by mass, max Max 12%w/w

Total Ash, percent by mass, on dry basis , max 8%

Acid insoluble Ash in dilute hydrochloric acid percent by mass, on dry basis , max Max 1.5%w/w

Solubility in cold water percent by mass, on dry basis , max Min 65%w/w

Bitterness expressed as direct reading of absorbance of picrocrocin at about 257 nm (on dry basis) Min 30%w/w

Safranal expressed as direct reading of absorbance of 330 nm (on dry basis) 20-50% w/w

Colouring strength expressed as direct reading of absorbance of 440 nm (on dry basis) Min 80% w/w

Total Nitrogen, percent by mass on dry basis, max 2

Floral waste percent by mass, max 10

Extraaneous matter percent by mass, max 1%

Purity test by TLC or paper chromato graphy Pure

Crude fiber on dry basis, ,ax 6% by wt.

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Aflatoxin B1 ppb ≤ 5

Aflatoxin (Total) ppb ≤10

Total Plate Count in 1 gm Max 100000

Yeast & mould in 1 gm Max 1000

E.Coli in 1 gm Absent

Salmonella in 25 gm Absent

Lead As Pb ppm Max 2.5

Arsenic as As ppm Max 1.1

Cadmium as Cd ppm Max 1.5

Mercury As Hg ppm Max 1.0

12 SMP Moisture Not more than 5% As per FSSA, 2006 and Rules & Regulations 2011

Milk Fat Not more than 1.5% m/m

Milk Protein in milk solids not Fat Not less than 34% m/m

Titrable Acidity (ml 0.1N NaOH/10gm solids not Fat Not more than 18

Insolubility index Max 1 ml

Total Ash on dry weight basis Not more than 8.2%

Scorched Particles Disc A/B only

Melamine Absent

TPC in 1 gm NMT 30,000

Coliform count in 1 gm NMT 10

E.Coli in 1 gm Absent

Yeast and Mould in 1 gm NMT 50

Salmonella in 25 gm Absent

S.aureus in 1 gm Absent

B.cereus in 1 gm NMT 500

Sulphite Reducing Clostridia in 1 gm NMT 50

Listeria monocytogens in 1 gm Absent

Lead as Pb ppm 0.02

Arsenic as As ppm 0.1

Cadmium as Cd ppm 0.02

Mercury As Hg ppm 0.01

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Antibiotic residues Absent

Aflatoxin M1 ppb ≤0.05

12 Sugar Sucrose ,% by Wt NLT 99.5 % As per FSSA, 2006 and Rules & Regulations 2011

Loss on Drying , % by Wt NMT 0.04

Total Ash (Sulphated ash) Max 0.10%

Reducing sugars NMT 0.04

Colour (ICUMSA Units) NMT 60

Sulphur Dioxide NMT 10

Lead As Pb ppm 0.5

Arsenic as As ppm 0.5

Copper as Cu ppm 2

Total Plate Count in 1 gm Max 200

Yeast & mould in 1 gm Max 100

E.Coli in 1 gm Absent

Salmonella in 25 gm Absent

13 Liquid Glucose Total solid(%by mass) Min. 80 As per FSSA, 2006 and Rules & Regulations 2011

Dextrose Qquivalent As declared

Reducing sugars (As Dextrose,dry bais) Min 30%w/w

Ash (% by mass) Max.0.3

Chloride Max 0.1%

Sulphated ash Max 0.3%

Colour (ICUMSA Units) Max 400 IU

Hydroxymethyl Fulphural (HMF) Max 40 mg/kg

Sulphur Dioxide mg/kg Max 40

Total Plate count in 1 gm Max 1000

Yeast & mould in 1 gm Max 100

E.coli, in 20 gm Absent

Salmonella in 20 gm Absent

14 Cone biscuit Moisture content ,% by Wt Max 5% As per FSSA, 2006 and Rules & Regulations 2011

Acid Insoluble Ash,% by Wt Max 0.1%

Total Ash% Max 2.0%

Total Plate count in 1 gm Max 10000 CFU

Yeast & mould in 1 gm Max 100 CFU

E.coli in 1 gm Absent

staphylococcus aureus in 1 gm Absent

Salmonella in 25 gm Absent

Lead As Pb ppm Max 2.5

Arsenic as As ppm Max 1.1

Copper ppm Max 30

Organochlorine Pesticides As per FSSR MRLs

Organophosphorous Pesticides As per FSSR MRLs

Synthetic pyrethroids As per FSSR MRLs

Banned Pesticides Absent

Total Aflatoxin ppb Max 15

Aflatoxin B1 ppb Max 10

15 Coffee Moisture on dry basis Not more than 5.0% As per FSSA, 2006 and Rules & Regulations 2011

Total Ash on dry basis Not more than 12.0%

Acid insoluble ash(on dry basis) Max 0.1%

Caffeined content on dry basis Not less than 2.8%

Solubility in boiling water in 1 gm Dissolves readily in 30 sec with moderate stirring

Solubility in cold water at 16 +/-2'C in 1 gm Soluble in 3 min with moderate stirring

Total Plate count in 1 gm Max 10000 CFU

Yeast & mould in 1 gm Max 100 CFU

Salmonella in 25 gm Absent

E.coli in 1 gm Absent

S.aureus in 1 gm Absent

Lead As Pb ppm Max 1.0

Arsenic as As ppm Max 1.0

Cadmium as Cd ppm Max 1.0

Mercury As Hg ppm Max 0.1

Aflatoxin B1 ppb Max 5

Total Aflatoxin ppb Max 10

Pesticide residue As per FSSR MRLs

Ochratoxin Mas 5 ug/kg

16 Pineapple Tit-Bits Drained weight ,% by Wt NLT 50% As per GCMMF

Brix (Total solubles solid) Min 15' - 25'

Acidity of syrup as citric acid Max 0.3-0.8 %

Total Plate count in 1 gm Max 50

Sulphur Dioxide ppm Max 100 As per FSSA, 2006 and Rules & Regulatio

Yeast & mould in 1 gm Max 100 CFU

Salmonella in 25 gm Absent

E.coli in 1 gm Absent

S.aureus in 1 gm Absent

Lead As Pb ppm Max 1.0

Arsenic as As ppm Max 1.0

Tin as Sn ppm Max 250

Total Aflatoxin ppb Max 10

Pesticide residue As per FSSR MRLs

17 Dark Chocolate ( Dark Chocodip)/Chocochips Buttons (Dark) Total fat, on dry basis (% by weight, mini) 25 As per FSSA, 2006 and Rules & Regulatio

Cocoa solids (on moisture free and fat free basis) percent by wt. not less than 12

Acid Insoluble Ash (on moisture, fat & sugar free basis)%age by weight, not more than Not more than 0.2

methyl mercury 0.25

Ochratoxin-A ug/kg Max 5

Aflatoxin B1 ppb Max 5

Total Aflatoxin ppb Max 10

18 White Chocolate ( white Chocodip)/Chocochips Buttons (white) Total fat, on dry basis (% by weight, mini) 25 As per FSSA, 2006 and Rules & Regulatio

Milk fat (on dry basis) percent by weight, mini 2

Milk Solids (on moisture free and fat free basis)%age by weight , not less than 10.5

Cocoa solids (on moisture free and fat free basis) percent by wt. not less than 2.5 (Exclude in white choclate)

Acid Insoluble Ash (on moisture, fat & sugar free basis)%age by weight, not more than Not more than 0.2

methyl mercury 0.25

Ochratoxin-A ug/kg Max 5

Aflatoxin B1 ppb Max 5

Total Aflatoxin ppb Max 10

19 Cocoa Powder Fineness (pass throgh 200 mesh) 99.5% min As per FSSA, 2006 and Rules & Regulatio

Moisture content , by Wt Max 5%

Cocoa Butter by weight (On dry basis) NLT 20

pH of 10% solution 5.8-6.2

Acid Insoluble Ash by weight (on Moisture and fat-free basis) NMT 1

Lead As Pb ppm Max 1.0

Arsenic as As ppm Max 1.0

Mercury As Hg ppm Max 0.1

Cadmium as Cd ppm Max 0.5

Total plate count/g in 1 gm Max 10000 cfu

Yeast & mould in 1 gm max 100 cfu

staphylococcus aureus in 1 gm absent

E-coli in 1 gm absent

salmonella in 25 gm absent

Aflatoxin B1 ppb Max 5

Total Aflatoxin ppb Max 10

Ochratoxin-A ug/kg Max 5

20 Flavours Diethylene Glycol Absent (shall not be used as solvent in flavours) As per FSSA, 2006 and Rules & Regulatio

Monoethyl Ether Absent (shall not be used as solvent in flavours)

Lead As Pb ppm Max 2

Arsenic as As ppm Max 3

Mercury as Hg ppm Max 1

Cadmium as Cd ppm Max 1

Total Plate count in 1 gm Max 10000 CFU

Yeast & mould in 1 gm Max 100 CFU

salmonella in 25 gm Absent

S.aureus in 1 gm Absent

E.Coli in 1 gm Absent

21 Colour - Tartrazine Colour/ Carmoisine supra Total dye content, corrected for sample dried at 105+/-1'C for 2 hours,percent by mass, mini 87 As per FSSA, 2006 and Rules & Regulatio

Loss on drying at 135'C, percent by mass, Max and chlorides and sulphates expressed as sodium salt, percent by mass, Max 13

Water insoluble matter,percent by mass, Max 0.2

Combined ether extracts, percent by mass, Max 0.2

Subsidiary dyes, percent by mass, Max 1

Dye intermediates, percent by mass, Max 0.5

Lead, mg/kg, Max 10

Arsenic, mg/kg, Max 3

Heavy Metals, mg/kg, Max 40

Aromatic amines Absent

Aromatic nitro compounds Absent

Aromatic hydrocarbons Absent

Cyanides Absent

22 Colour -Sunset yellow Colour Total dye content, corrected for sample dried at 105+/-1'C for 2 hours,percent by mass, mini 87 As per FSSA, 2006 and Rules & Regulatio

Loss on drying at 135'C, percent by mass, Max and chlorides and sulphates expressed as sodium salt, percent by mass, Max 13

Water insoluble matter,percent by mass, Max 0.2

Combined ether extracts, percent by mass, Max 0.2

Subsidiary dyes, percent by mass, Max 3

Dye intermediates, percent by mass, Max 0.5

Lead, mg/kg, Max 10

Arsenic, mg/kg, Max 3

Heavy Metals, mg/kg, Max 40

Aromatic amines Absent

Aromatic nitro compounds Absent

Aromatic hydrocarbons Absent

Cyanides Absent

23 Colour - Ponceau 4 R/ Carmoisine supra Total dye content, corrected for sample dried at 105+/-1'C for 2 hours,percent by mass, mini 85 As per FSSA, 2006 and Rules & Regulatio

Loss on drying at 135'C, percent by mass, Max and chlorides and sulphates expressed as sodium salt, percent by mass, Max 18

Water insoluble matter,percent by mass, Max 0.2

Combined ether extracts, percent by mass, Max 0.2

Subsidiary dyes, percent by mass, Max 1

Dye intermediates, percent by mass, Max 0.5

Lead, mg/kg, Max 10

Arsenic, mg/kg, Max 3

Heavy Metals, mg/kg, Max 40

Aromatic amines Absent

Aromatic nitro compounds Absent

Aromatic hydrocarbons Absent

Cyanides Absent

24 Colour-Erythrosine Total dye content, corrected for sample dried at 105+/-1'C for 2 hours,percent by mass, mini 87 As per FSSA, 2006 and Rules & Regulatio

Loss on drying at 135'C, percent by mass, Max and chlorides and sulphates expressed as sodium salt, percent by mass, Max 13

Water insoluble matter,percent by mass, Max 0.2

Ether extractable matter (alkaline), percent by mass, Max 0.2

Inorganic Iodide, percent by mass as sodium iodide, Max 0.1

Subsidiary colouring matters except fluorescein, percent by mass, Max 4

Fluoresence mg/kg Max 20

Organic compounds other than colouring matter 0.2

(a) Tri-iodoresorcinol,percent by mass, Max 0.2

(b) (2,4-dihydroxy-3, 5-di-iodobenzoyl) benzoic acid, percent by mass. Max, 0.2

Lead, mg/kg, Max 10

Arsenic, mg/kg, Max 3

Zinc, mg/kg, Max 50

Heavy Metals, mg/kg, Max 40

Aromatic amines Absent

Aromatic nitro compounds Absent

Aromatic hydrocarbons Absent

Cyanides Absent

25 Colour - Caramel Colour Total dye content, corrected for sample dried at 105+/-1'C for 2 hours,percent by mass, mini 87 As per FSSA, 2006 and Rules & Regulation

Loss on drying at 135'C, percent by mass, Max and chlorides and sulphates expressed as sodium salt, percent by mass, Max 13

Water insoluble matter,percent by mass, Max 0.2

Combined ether extracts, percent by mass, Max 0.2

Subsidiary dyes, percent by mass, Max 1

Dye intermediates, percent by mass, Max 0.5

Total Sulphur percent by mass 1.3-2.5

Sulphur Dioxide Max 0.2%

Total Nitrogen percent by mass max 0.2

Lead, mg/kg, Max 5

Arsenic, mg/kg, Max 3

Heavy Metals, mg/kg, Max 25

Mercury, mg/kg, Max 0.1

Copper, mg/kg, Max 20

Aromatic amines Absent

Aromatic nitro compounds Absent

Aromatic hydrocarbons Absent

Cyanides Absent

25 Citric Acid Water insoluble matter , ppm Max 30 Complete Analysis As Per IS 13186:1991 (RA 2020)

Chloride, ppm Max 5

Calcium , ppm Max 25

Tridodecylamine , ppm Max 0.1

Arsenic , mg/kg Max 3

Lead , mg/kg Max 0.5

26 Refined Coconut oil (Odorless) Moisture & Impurities % max 0.1 As per FSSA, 2006 and Rules & Regulation

B. R. reading at 40'C 34-35.5

Refractive Index at 40'C 1.4481 to 1.4490

Specific gravity at 30’C 0.915 to 0.920

Unsaponifiable matter Max. 1.0

Acid value Max. 0.5

Test of argemone oil Negative

Hexane content Max. 5.00 ppm

Saponification value Not less than 250

Iodine Value 7.5 to 10

Polenske Value Not less than 13

Total plate count/g, max 5000

Coliform/g max Absent

Yeat & Mould/g max Absent

27 Alphanso Mango Pulp Total Soluble Solids (Brix) 14 -25 ' As per FSSA, 2006 and Rules & Regulation

Acidity (as citric acid) Min 0.3

Acid insoluble ash % by wt Max 0.5

pH Value 3.5-4.2

Total plate count/g, max Max 10000 CFU

Yeat & Mould/g max Max 100 CFU

Coliform/0.1g Absent

Salmonella/25g Absent

E.Coli/25 g Absent

Lead as Pb ppm Max 1

Arsenic as As ppm Max 1.1

Copper as Cu ppm Max 5

Tin as Sn ppm Max 250

Cadmium as Cd ppm Not Specified

Mercury as Hg ppm Not Specified

methyl mercury ppm Not Specified

28 Fruit Preaparation Drain Weight Solid pack - Not Less than 70% of net wt. of contents As per FSSA, 2006 and Rules & Regulation

Total Ash Max 0.5%

Sulphur Dioxide Max 100

S.aureus in 25 gm Absent

Salmonella in 25 gm Absent

Shigella in 25 gm Absent

Clostridium botulinum in 25 gm Absent

E.coli in 1 gm Absent

Vibrio cholera in 25 gm Absent

Aflatoxin (Total) ppb 15

Coliform/g max in 1 gm Less than or equal to 10

Yeat & Mould/g max in 1 gm Less than or equal to 20

TPC/ml in 1 gm Not more than 50

Arsenic ppm Max 1.1

methyl mercury ppm Max 0.25

29 Fruit Compound TSS - Not less than -15% As per FSSA, 2006 and Rules & Regulation

Acidity as citric acid - NLT 0.3%

Fruit content Min. 25%

Arsenic ppm Max 1

S.aureus in 25 gm Absent

Salmonella in 25 gm Absent

Shigella in 25 gm Absent

Clostridium botulinum in 25 gm Absent

E.coli in 1 gm Absent

Vibrio cholera in 25 gm Absent

Aflatoxin (Total) ppb 15

Coliform/g max in 1 gm Less than or equal to 10

Yeat & Mould/g max in 1 gm Less than or equal to 20

TPC/g max in 1 gm Not more than 50

30 Honey Presence of colour, vitamins, minerals and saccharin Absent As per FSSA, 2006 and Rules & Regulation

Specific gravity at 27’C Not less than 1.35

Moisture Not more than 20% by mass

Total reducing sugars Not less than 65% by mass

Sucrose Not more than 5% by mass

Fructose-Glucose ratio 0.95-1.50

Ash Not more than 0.5% by mass

Acidity expressed as formic acid % by mass Max 0.20

Free Acidity Miliequivalents acid/1000 g ,Max 50

Water insoluble matters percent by mass,max 0.1

C-4 sugar,percent by mass,max 7

Fiehe’s test Negative

Hydroxy methyl furfural (HMF), mg/kg Not more than 80

2-Acetylfluran-3-Glucopyranoside (2-AFGP) as marker for rice syrup Absent

Proline , mg/kg Min. 180

Foreign Oligosaccharide (Max. Percent Peak) 0.7

Total count of pollens and plant elements/g of honey, 5000 Max

Optical density, at 660 nm, 0.3% Max

31 Cardamom Powder Moisture NMT 11% By Wt As per FSSA, 2006 and Rules & Regulation

Total Ash on dry basis NMT 8% By Wt

Ash insoluble in dilute HCL on dry basis NMT 3% By Wt

volatile oil content on dry basis NLT 3% by V/W

32 Caramel Cookies Ash insoluble in dilute HCL on dry basis shall not be more than 0.1 percent As per FSSA, 2006 and Rules & Regulation

Total Plate count/g Max 50000

Yeast and mold/g Max 100

Coliform count/g Absent

Salmonella/25g Absent

staphylococcus aureus/g Absent

E.coli/g Absent

Lead Max 0.5 ppm

Arsenic Max 0.1 ppm

Cadmium Max 0.1 ppm

Mycotoxins (Aflatoxin B1 and Total) Max 15 ug/kg

33 Fructo-Oligo-Sachharides (FOS) %moisture, max 25 As per FSSA, 2006 and Rules & Regulation

Fructo-oligo-sachharides, min 95

Glucose/Fructose/Sucrose, max 5

Total heavy metals, ppm, max 10

Arsenic, ppm, max 5

Lead, ppm, max 10

Copper, ppm, max 20

Coliform, max Absent in 0.1 g

Yeast & Mould count, max 200 cfu/g

Total plate count/g, max 1000

34 Sucralose Sucralose Assay calculated on anhydrous basis (%) 98-102 Complete Testing as per IS:15969-2013 (Reff 2020)

Methanol (%) max 0.1

Residue on idnition (Sulphated Ash), max 0.7

Water moisture, Max % 0.2

Arsenic (As), ppm, max 3

Lead as Pb, ppm, max 10

35 Dextrose/polydextrose Sulphated Ash NMT 0.1% ON DRY BASIS As per FSSA, 2006 and Rules & Regulation

Acidity 0.5gm dissolved in 50 ml of boiled and cooled water requires for neutralize NMT 0.20ml of N/10 sodium hydroxide to ohenolphthalein indicator

D-Glucose NLT 99.0% ON DRY BASIS

Moisture Max.9.5%

36 Orange crush Fruit juice,min(%) 25.00% As per FSSA, 2006 and Rules & Regulation

Total solid min (%) 55

Acidity of extracted as citric acid,max(%) 3.5

coliform/g ,max absent

Yeast and mould count/g,max 100 cfu/g

37 Orange Jelly Fruit juice /puree in final product min % 45% As per FSSA, 2006 and Rules & Regulation

TPC not more than 50cfu/ml

Yeast & mould count not more than 2.0cfu/ml

Coli form Absent in 100ml

Flat Sour organism not more than 10000 cfu/gm for those product which has pH less than 5.2

total soluble solid Min (%) 65

Acidity of extracted as citric acid max(%) 3.5

38 Maltodextrin Moisture %, Max 5 FSSA, 2006 and Rules & Regulations 2011

Bulk Density loose, GLI 440-560

Bulk Density packed, GLI 520-640

Dextrose Equivalent % 16.00-19.90

Granulometry>400 micron % 7

Granulometry<63 micron % 35

Sulphur dioxide, ppm 10

Total Plate count/g, CFU 500

Yeasts & Moulds/g, CFU 100

Salmonella/25g Absent

E. coli/g Absent

Apparent starch Pass

39 Culture Coagulase-positive staphylococci in 1 gm Absent As per FSSA, 2006 and Rules & Regulation

Non lactic acid bacteria in 1 gm less than 500

Enterobacteracea in 1 gm Absent

Coliform count in 1 gm Absent

E. coli in 1 gm Absent

Shigella in 25 gm Absent

Salmonella in 25 gm Absent

S. aureus in 1 gm Absent

Yeast and Mould in 1 gm Absent

Listeria monocytogens in 25 gm Absent

40 Wooden stick/spoon Enterobacteracea in 1 gm Absent As per FSSA, 2006 and Rules & Regulation

TPC in 1 gm < 10

Coliform count in 1 gm Absent

E. coli in 1 gm Absent

Shigella in 25 gm Absent

Salmonella in 25 gm Absent

S. aureus in 1 gm Absent

Yeast and Mould in 1 gm Absent

Listeria monocytogens in 25 gm Absent

Aflatoxin µg/kg 15

41 Chocolate Brownie Moisture, % 12.00-17.00 As per FSSA, 2006 and Rules & Regulation

Coliform in 1 gm Absent

SPC, Max in 1 gm 1000

Yeast & Mold in 1 gm Absent

42 Sweetened condensed milk (SCM) Moisture, % Max 27 As per FSSA, 2006 and Rules & Regulation

Milk Fat (%) Min 8

Milk solid not Fat (%) Min 20

Total Milk Solids(%) Min 28

Added sugar (Sucrose%) Min 40

Total Solids(%) Min 73

Protein(%) Min 7

Titratable acidity(as lactic acid) Max 0.25%

Ash (%) As per specification

Total Plate Count in 1 gm Max 20000 CFU

E.Coli in 1 gm Absent

Coliform in 0.1 gm Absent

Yeast & Mold in 1 gm Max 100 CFU

S.aureus in 1 gm Absent

Salmonella in 25 gm Absent

Aflatoxin M1 ug/kg Max 0.5

Melamine mg/kg Absent

Antibiotic residues Absent

Pesticide residues Absent

Lead as Pb ppm Max 0.02

Arsenic as As ppm Max 0.1

Cadmium as Cd ppm Max 0.02

Mercury as Hg ppm Max 0.01

43 Fatty Acid Profile of ghee sample

Packaging Material

S.N. Sample Description Test Parameters Unit Specified Norms Reference Rate (Basic)

1 Milk polyfilms including UHT milk polyfim/Ice candy Laminates/Ice cream laminates/Ice cream cup/container/tub/Ice cream cartons Fermented products polyfil/cup/container/mataka Overall Global Migration with all stimulants (Ethanol. Acetic acid, n-Heptane & Distilled water) Distt water 10 mg/dm2 IS 9845 : 1998 (reaffiremed 2020)

10% Ethanol 10 mg/dm2

n-Heptane 10 mg/dm2

3% Acetic Acid 10 mg/dm2

Specific Migration limit

Substances Max. Migration Limit As per FSSA, 2006 and Rules & Regulations 2011

Cobalt mg/kg 0.05

Lithium mg/kg 0.6

Manganese mg/kg 0.6

Antimony mg/kg 0.04

Phthalic acid, bis (2- ethylhexyl) ester (DEHP) mg/kg 1.5

2 LIDS / FOILS Global Migration Test from printed and stamped side mg/dm2 10 IS 9845 : 1998 (reaffiremed 2020)

S.N. Sample Description Test Parameters Specified Norms Reference Rate (Basic)

1 Raw water/Process water as per IS :10500-2012 Table 1 Organoleptic and Physical Parameters

i) Colour IS 3025 Part 4

ii) Odour IS 3025 Part 5

iii) pH value IS 3025 Part 11

iv) Taste IS 3025 Part 7 and 8

v) Turbidity, IS 3025 Part 10

vi) Total dissolved solids IS 3025 Part 16

Table 2 General Parameters Concerning Substances Undesirable in Excessive Amounts

i) Aluminium IS 3025 (Part 55)

ii) Ammonia (as total ammonia-N) IS 3025 (Part 34)

iii) Anionic detergents (as MBAS) Annex K IS 13428

iv) Barium Annex F IS 13428

v) Boron IS 3025 (Part 57)

vi) Calcium IS 3025 (Part 40)

vii) Chloramines IS 3025 (Part 26)

viii) Chloride IS 3025 (Part 32)

ix) Copper IS 3025 (Part 42)

x) Fluoride IS 3025 (Part 60)

xi) Free residual chlorine IS 3025 (Part 26)

xii) Iron IS 3025 (Part 53)

xiii) Magnesium IS 3025 (Part 46)

xiv) Manganese IS 3025 (Part 59)

xv) Mineral oil Clause 6 IS 3025 — (Part 39) Infrared Partition method

xvi) Nitrate (as NO3), IS 3025 (Part 34)

xvii) Phenolic compounds (as C6H5OH), IS 3025 (Part 43)

xviii Selenium (as Se), IS 3025 (Part 56) or IS 15303

xix) Silver Annex J IS 13428

xx) Sulphate IS 3025 (Part 24)

xxi) Sulphide IS 3025 (Part 29)

xxii) Total alkalinity as calcium carbonate IS 3025 (Part 23)

xxiii Total hardness (as CaCO3) IS 3025 (Part 21)

xxiv Zinc IS 3025 (Part 49)

Table 3 Parameters Concerning Toxic Substances

i) Cadmium IS 3025 (Part 41)

ii) Cyanide IS 3025 (Part 27)

iii) Lead IS 3025 (Part 47)

iv) Mercury IS 3025 (Part 48)/ Mercury analyser

v) Molybdenum IS 3025 (Part 2)

vi) Nickel IS 3025 (Part 54)

vii) Polychlorinated biphenyls ASTM 5175

viii) Polynuclear aromatic hydrocarbons (as PAH) APHA 6440

ix) Total arsenic IS 3025 (Part 37)

x) Total chromium IS 3025 (Part 52)

xi) Trihalomethanes

a) Bromoform ASTM D 3973-85 or APHA 6232

b) Dibromochlorometh ane ASTM D 3973- 85or APHA 6232

c) Bromodichlorometh ane ASTM D 3973- 85or APHA 6232

d) Chloroform ASTM D 3973- 85or APHA 6232

E) Uranium No Relaxation

Table 4 Parameters Concerning Radioactive Substances

i) Alpha emitters IS 14194 Part 2

ii) Beta emitters IS 14194 Part 1

Table 5 Pesticide Residues

i) Alachlor USEPA 525.2, 507

ii) Atrazine USEPA 525.2, 8141 A

iii) Aldrin/ Dieldrin USEPA 508

iv) Alpha HCH USEPA 508

v) Beta HCH USEPA 508

vi) Butachlor USEPA 525.2, 8141 A

vii) Chlorpyriphos USEPA 525.2, 8141 A

viii) Delta HCH USEPA 508

ix) 2,4- Dichlorophenoxyac etic acid USEPA 515.1

x) DDT (o, p and p, p – isomers of DDT, DDE and DDD) USEPA 508 OR AOAC 990.06

xi) Endosulfan (alpha, beta, and sulphate) USEPA 508 OR AOAC 990.06

xii) Ethion USEPA 1657 A

xiii) Gamma — HCH (Lindane) USEPA 508 OR AOAC 990.06

xiv) Isoproturon USEPA 532

xv) Malathion USEPA 8141 A

xvi) Methyl parathion USEPA 8141 A OR ISO 10695

xvii) Monocrotophos USEPA 8141 A

xviii) Phorate USEPA 8141 A

Table 6 Bacteriological Quality of Drinking Water

i) E. coli or thermotolerant coliform bacteria IS 15185

ii) Total coliform bacteria IS 15185

ii) Algae IS 15185

ii) Toxin producing organism IS 15185

4.2 Virological Requirements

i) MS2 phage USEPA method 1602

ii) Polymerase Chain Reaction (PCR) method Annex B IS 10500 or USEPA method in Manual of Method for Virology Chapter 16, June 2001

4.3 Biological Requirements

i) Flagellates IS 10500

i) Zooplanktons IS 10500

ii) Cryptosporidium USEPA method 1622 or USEPA method 1623* or ISO 15553 : 2006

iii) . Giardia USEPA method 1623* or ISO 15553 : 2006

2 Chilled water sample from cold well and cooling tower Detection and enumeration of Legionella sp Absent As per IS 11731:1999

S.N. Sample Description Test Parameters Specified Norms Reference Rate (Basic)

1 Compressed Air used in ice cream (As per ISO-8573 part 1) Number of Particle per m3 Max 6000 As per ISO-8573 part 1

Total Fungal count NA

Hydrocarbons NA

Dew Point Max -40

Oil & mist Max 1

Total Viable count NA