Annual Rate contract for Testing of Milk and Milk Products through External NABL Laboratory at Dudhmoti sagar Dairy Dharuhera

Pasteurized milk pouch:

Fat determination by Rose-Gottlieb Method

Milk Solids Not Fat determination by AOAC 990:21 Method

Reichert Meissl value (Extracted Fat)

BR Test at 40 deg C (Extracted Fat)

Mineral Oil (Extracted Fat)Test

Foreign fat (Extracted Fat)

Detection of Sugar

Detection of Neutralizers

Detection of Starch

Detection of Sodium Chloride Test

Detection of Nitrates (Pond Water)Test

Presence of Sodium Thiosulphate

Detection of Ammonium Compounds

Presence of Sulphates

Estimation of Urea

Presence of Formalin

Presence of Boric acid and Borates

Detection of Hypochlorites and Chloramines

Detection of Maltodextrin

Detection of Added Glucose

Presence of Anionic Detergent

Detection of Cellulose

Test for Quaternary Ammonium Compounds

Detection of Gelatine

Presence of Hydrogen Peroxide

Presence of Salicylic acid

Presence of Skimmed milk Powder

Sodium Content, mg/100g SNF

Potassium Content, mg

Other Contaminants

Microbiological Parameter

Aerobic Plate Count

Listeria monocytogens

Metal Contaminants

1. Chlorpyriphos

2. Ethion (Residues to be determined as ethion and Its oxygen analogue and expressed as ethion)

3. Monocrotophos

5. Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate)

6. Pirimiphos-methyl

7. Paraquat Dichloride (Determined as Paraquat cations)

9. Sum of benomyl and carbendazim expressed as carbendazim

10. Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran

13. 2,4-Dichlorophenoxy Acetic Acid

14. Acephate (expressed as mixture Methamidophos and acephate)

15. Acetamiprid

16. Azoxystrobin

21. Chlorantraniliprole

22. Chlorothalonil

23. Chlothianidin (Chlothianidin and its metabolites

Thiazolymethylguanidine (TMG),Thiazolymethylurea (TZMU),

Methylnitroguanidine (MNG)

24. Deltamethrin (Decamethrin)

25. Dichlorvos (DDVP) (content of di-chloroacetaldehyde (D.C.A.) be

reported where possible)

26. Difenoconazole

28. Dinotefuran

30. Metiram as CS2

31. Emamectin Benzoate

32. Ethofenprox (Etofenprox)

33. Fenpropathrin

35. Flubendiamide

36. Flusilazole

37. Glufosinate Ammonium

38. Imidacloprid

40. Kresoxim Methyl

42. Methyl Chlorophenoxy Acetic Acid (MCPA)

43. Metolachlor

44. Oxydemeton-Methyl

45. Penconazole

46. Propiconazole

47. Pyraclostrobin

48. Tebuconazole

49. Thiacloprid

50. Thiamethoxam

51. Thiophanate-Methyl

52. Triacontanol

53. Triadimefon

54. Cypermethrin (sum of isomers) (fat soluble residue)

55. Fenvalerate (fat soluble residue)

NUTRITIONAL PARAMETER:

2.Total Carbohydrate,g

3.Added Sugar,g

5.Saturated Fat,g

7. Cholesterol (mg)

Antibiotic Residues

Chlortetracycline/Oxytetracycline/Tetracycline

Febantel/Fenbendazole/Oxyfendazole

Sulphaquinoxaline

SulfaChloropyrazine

Raw Chilled milk :

Fat determination by Rose-Gottlieb Method

Milk Solids Not Fat determination by AOAC 990:21 Method

Reichert Meissl value (Extracted Fat)

BR Test at 40 deg C (Extracted Fat)

Mineral Oil (Extracted Fat)Test

Foreign fat (Extracted Fat)

Detection of Sugar

Detection of Neutralizers

Detection of Starch

Detection of Sodium Chloride Test

Detection of Nitrates (Pond Water)Test

Presence of Sodium Thiosulphate

Detection of Ammonium Compounds

Presence of Sulphates

Estimation of Urea

Presence of Formalin

Presence of Boric acid and Borates

Detection of Hypochlorites and Chloramines

Detection of Maltodextrin

Detection of Added Glucose

Presence of Anionic Detergent

Detection of Cellulose

Test for Quaternary Ammonium Compounds

Detection of Gelatine

Presence of Hydrogen Peroxide

Presence of Salicylic acid

Presence of Skimmed milk Powder

Potassium Content

Other Contaminants

Metal Contaminants

1. Chlorpyriphos

2. Ethion (Residues to be determined as ethion and Its oxygen analogue and expressed as ethion)

3. Monocrotophos

5. Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate)

6. Pirimiphos-methyl

7. Paraquat Dichloride (Determined as Paraquat cations)

9. Sum of benomyl and carbendazim expressed as carbendazim

10. Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran

13. 2,4-Dichlorophenoxy Acetic Acid

14. Acephate (expressed as mixture Methamidophos and acephate)

15. Acetamiprid

16. Azoxystrobin

21. Chlorantraniliprole

22. Chlorothalonil

23. Chlothianidin (Chlothianidin and its metabolites

Thiazolymethylguanidine (TMG),Thiazolymethylurea (TZMU),

Methylnitroguanidine (MNG)

24. Deltamethrin (Decamethrin)

25. Dichlorvos (DDVP) (content of di-chloroacetaldehyde (D.C.A.) be

reported where possible)

26. Difenoconazole

28. Dinotefuran

30. Metiram as CS2

31. Emamectin Benzoate

32. Ethofenprox (Etofenprox)

33. Fenpropathrin

35. Flubendiamide

36. Flusilazole

37. Glufosinate Ammonium

38. Imidacloprid

40. Kresoxim Methyl

42. Methyl Chlorophenoxy Acetic Acid (MCPA)

43. Metolachlor

44. Oxydemeton-Methyl

45. Penconazole

46. Propiconazole

47. Pyraclostrobin

48. Tebuconazole

49. Thiacloprid

50. Thiamethoxam

51. Thiophanate-Methyl

52. Triacontanol

53. Triadimefon

54. Cypermethrin (sum of isomers) (fat soluble residue)

55. Fenvalerate (fat soluble residue)

Antibiotic Residues

Chlortetracycline/Oxytetracycline/Tetracycline

Febantel/Fenbendazole/Oxyfendazole

Sulphaquinoxaline

SulfaChloropyrazine

Buttermilk/Masala buttermilk/Sweet Lassi :

Microbiological Parameter

Yeast and Mould

Listeria monocytogens

Probiotic Count (Lactobacillus spp., Bifidobacterium spp.)

Lactic Acid Bacterial count not applicable for Sweet Lassi

Metal Contaminants

1. Chlorpyriphos

2. Ethion (Residues to be determined as ethion and Its oxygen analogue and expressed as ethion)

3. Monocrotophos

5. Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate)

6. Pirimiphos-methyl

7. Paraquat Dichloride (Determined as Paraquat cations)

9. Sum of benomyl and carbendazim expressed as carbendazim

10. Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran

13. 2,4-Dichlorophenoxy Acetic Acid

14. Acephate (expressed as mixture Methamidophos and acephate)

15. Acetamiprid

16. Azoxystrobin

21. Chlorantraniliprole

22. Chlorothalonil

23. Chlothianidin (Chlothianidin and its metabolites

Thiazolymethylguanidine (TMG),Thiazolymethylurea (TZMU),

Methylnitroguanidine (MNG)

24. Deltamethrin (Decamethrin)

25. Dichlorvos (DDVP) (content of di-chloroacetaldehyde (D.C.A.) be

reported where possible)

26. Difenoconazole

28. Dinotefuran

30. Metiram as CS2

31. Emamectin Benzoate

32. Ethofenprox (Etofenprox)

33. Fenpropathrin

35. Flubendiamide

36. Flusilazole

37. Glufosinate Ammonium

38. Imidacloprid

40. Kresoxim Methyl

42. Methyl Chlorophenoxy Acetic Acid (MCPA)

43. Metolachlor

44. Oxydemeton-Methyl

45. Penconazole

46. Propiconazole

47. Pyraclostrobin

48. Tebuconazole

49. Thiacloprid

50. Thiamethoxam

51. Thiophanate-Methyl

52. Triacontanol

53. Triadimefon

54. Cypermethrin (sum of isomers) (fat soluble residue)

55. Fenvalerate (fat soluble residue)

NUTRITIONAL PARAMETER

2.Total Carbohydrate,g

3.Added Sugar,g

5.Saturated Fat,g

7. Cholesterol (mg)

9.Salt (NaCl),mg For Masala Butter milk

Other Contaminants

Total Aflatoxin For Masala Butter milk

Masti Dahi/Low fat Dahi/TM Dahi/Lactose free dahi :

Microbiological Parameter

Yeast and Mould

Listeria monocytogens

Lactic Acid Bacterial count

Metal Contaminants

1. Chlorpyriphos

2. Ethion (Residues to be determined as ethion and Its oxygen analogue and expressed as ethion)

3. Monocrotophos

5. Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate)

6. Pirimiphos-methyl

7. Paraquat Dichloride (Determined as Paraquat cations)

9. Sum of benomyl and carbendazim expressed as carbendazim

10. Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran

13. 2,4-Dichlorophenoxy Acetic Acid

14. Acephate (expressed as mixture Methamidophos and acephate)

15. Acetamiprid

16. Azoxystrobin

21. Chlorantraniliprole

22. Chlorothalonil

23. Chlothianidin (Chlothianidin and its metabolites

Thiazolymethylguanidine (TMG),Thiazolymethylurea (TZMU),

Methylnitroguanidine (MNG)

24. Deltamethrin (Decamethrin)

25. Dichlorvos (DDVP) (content of di-chloroacetaldehyde (D.C.A.) be

reported where possible)

26. Difenoconazole

28. Dinotefuran

30. Metiram as CS2

31. Emamectin Benzoate

32. Ethofenprox (Etofenprox)

33. Fenpropathrin

35. Flubendiamide

36. Flusilazole

37. Glufosinate Ammonium

38. Imidacloprid

40. Kresoxim Methyl

42. Methyl Chlorophenoxy Acetic Acid (MCPA)

43. Metolachlor

44. Oxydemeton-Methyl

45. Penconazole

46. Propiconazole

47. Pyraclostrobin

48. Tebuconazole

49. Thiacloprid

50. Thiamethoxam

51. Thiophanate-Methyl

52. Triacontanol

53. Triadimefon

54. Cypermethrin (sum of isomers) (fat soluble residue)

55. Fenvalerate (fat soluble residue)

NUTRITIONAL PARAMETER

2.Total Carbohydrate,g

3.Added Sugar,g

5.Saturated Fat,g

7. Cholesterol (mg)

Other Contaminants

Microbiological Parameter

Yeast and Mould

Listeria monocytogens

Lactic Acid Bacterial count

Metal Contaminants

1. Chlorpyriphos

2. Ethion (Residues to be determined as ethion and Its oxygen analogue and expressed as ethion)

3. Monocrotophos

5. Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate)

6. Pirimiphos-methyl

7. Paraquat Dichloride (Determined as Paraquat cations)

9. Sum of benomyl and carbendazim expressed as carbendazim

10. Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran

13. 2,4-Dichlorophenoxy Acetic Acid

14. Acephate (expressed as mixture Methamidophos and acephate)

15. Acetamiprid

16. Azoxystrobin

21. Chlorantraniliprole

22. Chlorothalonil

23. Chlothianidin (Chlothianidin and its metabolites

Thiazolymethylguanidine (TMG),Thiazolymethylurea (TZMU),

Methylnitroguanidine (MNG)

24. Deltamethrin (Decamethrin)

25. Dichlorvos (DDVP) (content of di-chloroacetaldehyde (D.C.A.) be

reported where possible)

26. Difenoconazole

28. Dinotefuran

30. Metiram as CS2

31. Emamectin Benzoate

32. Ethofenprox (Etofenprox)

33. Fenpropathrin

35. Flubendiamide

36. Flusilazole

37. Glufosinate Ammonium

38. Imidacloprid

40. Kresoxim Methyl

42. Methyl Chlorophenoxy Acetic Acid (MCPA)

43. Metolachlor

44. Oxydemeton-Methyl

45. Penconazole

46. Propiconazole

47. Pyraclostrobin

48. Tebuconazole

49. Thiacloprid

50. Thiamethoxam

51. Thiophanate-Methyl

52. Triacontanol

53. Triadimefon

54. Cypermethrin (sum of isomers) (fat soluble residue)

55. Fenvalerate (fat soluble residue)

NUTRITIONAL PARAMETER

2.Total Carbohydrate,g

3.Added Sugar,g

5.Saturated Fat,g

7. Cholesterol (mg)

Other Contaminants

Fat % (on dry basis, for paneer)

Protein % (on dry basis, for paneer)

Ash, percent by mass (on dry basis) for Paneer

Detection of Starch

Other Contaminants

Aflatoxin (Total)

Metal Contaminants

Microbiological Parameter

Yeast and Mould

Listeria monocytogens

Aerobic Plate Count

1. Chlorpyriphos

2. Ethion (Residues to be determined as ethion and Its oxygen analogue and expressed as ethion)

3. Monocrotophos

5. Phorate (sum of Phorate, its oxygen analogue and their sulphoxides and sulphones, expressed as phorate)

6. Pirimiphos-methyl

7. Paraquat Dichloride (Determined as Paraquat cations)

9. Sum of benomyl and carbendazim expressed as carbendazim

10. Carbofuran (sum of carbofuran and 3-hydroxy carbofuran expressed as carbofuran

13. 2,4-Dichlorophenoxy Acetic Acid

14. Acephate (expressed as mixture Methamidophos and acephate)

15. Acetamiprid

16. Azoxystrobin

21. Chlorantraniliprole

22. Chlorothalonil

23. Chlothianidin (Chlothianidin and its metabolites

Thiazolymethylguanidine (TMG),Thiazolymethylurea (TZMU),

Methylnitroguanidine (MNG)

24. Deltamethrin (Decamethrin)

25. Dichlorvos (DDVP) (content of di-chloroacetaldehyde (D.C.A.) be

reported where possible)

26. Difenoconazole

28. Dinotefuran

30. Metiram as CS2

31. Emamectin Benzoate

32. Ethofenprox (Etofenprox)

33. Fenpropathrin

35. Flubendiamide

36. Flusilazole

37. Glufosinate Ammonium

38. Imidacloprid

40. Kresoxim Methyl

42. Methyl Chlorophenoxy Acetic Acid (MCPA)

43. Metolachlor

44. Oxydemeton-Methyl

45. Penconazole

46. Propiconazole

47. Pyraclostrobin

48. Tebuconazole

49. Thiacloprid

50. Thiamethoxam

51. Thiophanate-Methyl

52. Triacontanol

53. Triadimefon

54. Cypermethrin (sum of isomers) (fat soluble residue)

55. Fenvalerate (fat soluble residue)

NUTRITIONAL PARAMETER

Total Carbohydrate,g

Saturated Fat,g

Cholesterol (mg)

Raw water : Sample should be analyzed as per IS-10500

1.Colour Hazen units,max

5.Turbidity,NTU,Max

6.Dissolved Solids mg/l,Max

7.Aluminium(as Al)mg/l,Max

8.Ammonia(as total ammonia N)

9.Anionic detergents(as MBAS)mg/l,Max"

10.Barium(as Ba)

11.Boron mg/l,Max

12.Calcium(as Ca)mg/l,Max

13.Chloramines(as Cl2)

14.Chloride(as Cl)mg/l,Max

15.Copper(as Cu)mg/l,Max

16.Fluoride(as F)mg/l,Max

17.Residual(Free Chlorine)mg/l,Min"

18.Iron(as Fe)mg/l,Max

19.Magnesium(as Mg)mg/l,Max"

20.Manganese(as Mn)mg/l,Max"

21.Mineral oil mg/l,Max

22.Nitrate(as NO3)

23.Phenolic Compounds(as C6H5OH)mg/l,Max

24.Selenium(as Se)mg/l,Max

25.Silver(as Ag)

26.Sulphate(as SO4)mg/l,Max"

27.Suphide(as H2S)

28.Total Alkanity as calcium carbonate"

29.Total Hardness as CaCO3

31.Cadmium(as Cd)mg/l,Max

32.Cyanide(as CN)mg/l,Max

33.Lead(as Pb)mg/l,Max

34.Mercury(as Hg)mg/l,Max

35.Molybdenum(as Mo)

36.Nickel(as Ni)

37.Polychlorinated biphenyls

38.Polynuclear aromatic hydrocarbons as(PAH)

39.Arsenic(as As)mg/l,Max

40.Chromium(as Cr6+)mg/l,Max"

Trihalomethanes

42.Dibromochloromethane

43.Bromodiechloromethane

Pesticide Residues as per table-5

Aldrin/Dieldrin

2,4-Dichlorophenoxyacetic acid

DDT (isomers of DDT), DDE and DDD

Endosulfan (alpha, beta and sulphate)

Gamma-HCH (Lindane)

Methyl parathion

Radio active residues

a) Alpha emitters µc/ml

b) Beta emitters µc/ml

Microbiological Parameter

E.Coli or Thermotolerant coliform bacteria

Total coliform bacteria

MS2 phage Optional (Infrequently)

Cryptosporidium

algae, zooplanktons,

flagellates, parasites and toxin producing organisms.

acrylamide content in water

Processed water : Sample should be analyzed as per IS-10500

Physical chemical characteristics

1. Colour (Hazen units), Max

2. Turbidity (Units),Max

5. Total solids mg/l,Max

6. Total hardness(as CaCO3)mg/l,Max

7. Sulphate (as SO4)mg/l,Max

8.Fluoride (as F)mg/l,Max

9. Chloride(as Cl)mg/l,Max

10. Cyanide (as CN)mg/l,Max

11. Selenium (as Se)mg/l,Max

12. Iron (as Fe)mg/l,Max

13. Magnesium (as Mg)mg/l,Max

14. Manganese (as Mn)mg/l,Max

15. Copper (as Cu)mg/l,Max

16.Lead (as Pb)mg/l,Max

17.Chromium (as Cr6+)mg/l,Max

18.Zinc (as Zn)mg/l,Max

19.Arsenic (as As)mg/l,Max

20.Nitrate (NO2)mg/l,Max

21.Phenolic Compounds (as C6H5OH )mg/l,Max

22. Cadmium (as Cd)mg/l,Max

23. Mercury (as Hg)mg/l max

Radio active residues

a) Alpha emitters µc/ml

b) Beta emitters µc/ml

Microbiological Parameter

Coliform bacteria,MPN index per 100ml

Proteolytic & Lipolytic organism combined count per ml Max

Thermophilic bacteria

Slime-forming organisms

acrylamide content in water

Packaging material :

1 a. Global migration test with simulants B & D as per IS 9845 (pH<5, acidic food): for Dahi,Buttermilk,Lassi packaging material

b. Global migration test with stimulants A & D as per IS 9845 (pH>5, nonacidic food): for Milk,Sweet packaging material

c. Global migration test with stimulants A,B & D as per IS 9845 {High temperature heat sterilized (Retorting) condition of use} for Paneer packaging material

2 Result of color migration for all packaging materials

3 specific migration of Phthalic Acid included

4 Metal Contaminants for all packaging materials

Common Sugar/Sucrose :

Complete testing as per IS 1151:2021 & FSSAI

Sucrose Content

Loss on drying, by mass

Reducing sugar, by mass

Colour in ICUMSA units

Conductivity ash by mass

Sulphur dioxide

Microbiological Parameter

Flat Sour Organisms

Clostridium botulinum

Yeast and Mould

Other Contaminants

Aflatoxin (Total)

Metal Contaminants

Sum of benomyl and carbendazim expressed as carbendazim

Ethion(Residues to be determined as ethion and its oxygen analogue and expressed as ethion)

Compostional Parameter

Extraneous matter

Total ash on dry basis

Volatile oil content on dry basis

Insect damaged matter

Added colouring matter

Compostional Parameter

Extraneous matter

Moisture and volatile matter

Ash insoluble %by mass

Solubility in cold water

Bitterness expressed as direct reading of absordance of picrocrosin at about 257 nm(on dry basis)

Safranal expressed as direct reading of absorbance of 330nm (on dry basis)

Colouring strength expressed as direct reading absorbance of 440nm (on dry basis)

Total nitrogen %by mass (on dry basis)

Crude fibre %by mass (on dry basis)

Added coluring matter

Mineral analysis

Flavour (seasoning) :

Compositional Parameter

Moisture (by weight)

Acid Insoluble Ash in dilute HCl (on dry basis)

Metal contaminants

Bromide (Determineed and expressed as total Bromide from all sources)

Microbiological Parameter

Other Contaminants

Total Aflatoxin

Flavour (Paste) for Tadka buttermilk :

Compositional Parameter

Diehthylene glycol

Monoethyl ether

Extraneous matter

Skim Milk Powder :

Compositional Parameter

Moisture, percent by mass

Total Solid percent by mass

Milk Protein in milk solid not fat, percent by mass

Fat, percent by mass

Scorched Particles

Insolubility Index, ml

Total Ash (on dry basis) percent by mass

Titratable acidity (lactic acid), percent by mass

Microbiological Parameter

Bacterial count, per gram

Coliform count, per gm

E.coli, per gram

Staphylococcus aureus per gram (Coagulase positive)

Salmonella per 25 gram

Listeria monocytogens, per gram

Anaerobic Spore count (Sulphite reducing clostridia)

Aerobic Spore count (Bacillus cereus)

Anaerobic Spore count (Clostridium perfringenes)

Other Contaminants

Metal Contaminants

Compositional Parameter

Taste and Flavour

Moisture, percent by mass

Milk fat, percent by mass

Free fatty acid as oleic acid, percent by mass

Butyro-Refractometer reading at 40°C

Reichert Meissl value

Peroxide value, milli-equivalent of oxygen per kg of sample

Presence of foreign fat (animal/vegetable)

BHA content < 0.02 %

Phenolphthalein test

Phytosteryl acetate test

Milk Fat Purity

Microbiological Parameter

Coliform count, per gm

MICROBIAL ANALYSIS OF MILK/MILK PRODUCTS AS REQUIRED

Aerobic Plate Count

Listeria monocytogens